苏丹红Ⅰ的单扫描极谱法测定

被引:5
作者
蒋雯菁 [1 ]
万渝平 [2 ]
黄荔 [2 ]
但德忠 [1 ]
机构
[1] 四川大学环境科学与工程系
[2] 成都市产品质量监督检验所
关键词
苏丹红Ⅰ; 单扫描极谱法; 添加剂; 食品安全;
D O I
暂无
中图分类号
TS207.3 [食品分析与检验];
学科分类号
100403 [营养与食品卫生学];
摘要
A novel method for determination of SudanⅠ in food by single scan polarography has been developed in this paper.It was found that a well-shape second derivation polarographic wave was observed at peak potential Ep-0.79V(vs.SCE)in the mediums of sodium tetraborate and ethanol.The peak current for the wave was proportional to concentration of Sudan I.The linear range was 0.1μg/mL1.6μg/mL.The coefficient of correlation was 0.9983.The detection limit of the method was 0.025μg/mL.Its relative standard deviation(RSD) was ≤1.1%(n=6).Average recoveries of blank were over the range of 88.0%~101.0% and average recoveries of pepper samples were over the range of 91.0%~117.4%.The proposed method is rapid,simple,accurate and highly sensitive,which provided the new gist to improving and perfecting the method for determination of SudanⅠ,and possessed a significant practical value.
引用
收藏
页码:1381 / 1384
页数:4
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