气质联用法测定医用橡皮塞中防老剂BHT

被引:7
作者
张伟亚
王成云
张少文
机构
[1] 深圳出入境检验检疫局,深圳出入境检验检疫局,洛阳大学广东深圳 ,广东深圳 ,河南洛阳
关键词
气质联用法; 医用橡皮塞; BHT;
D O I
暂无
中图分类号
TQ330 [一般性问题];
学科分类号
081705 [工业催化];
摘要
A new method for determination of 2,6-ditertbutyl-p-cresol in medical rubber plug by gas chromatography/mass spectrometry was developed.Analytical method and extraction conditions were optimized. Retention time and mass spectra of total ion chromatography were used for qualitative analysis. The m/z 205 was quantitative ion for BHT by gas chromatography/mass spectrometry/selected ion storage. The method is simple, rapid and accurate. The detection limit of BHT was 0.01mg/L,the recovery was 90.18~96.64% and the RSD(n=7) was 1.34%.
引用
收藏
页码:103 / 104
页数:2
相关论文
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[2]
气相色谱-质谱选择离子法测定化妆品中抗氧化剂丁基羟基茴香醚、二丁基羟基甲苯 [J].
张伟亚 ;
吴采樱 ;
王成云 ;
杨左军 ;
刘丽 .
色谱, 2002, (02) :178-181