土壤样品中多环芳烃的GC-MS快速分析方法

被引：5

作者：

佟玲 ^{[1
]}

周瑞泽 ^{[2
]}

吴淑琪 ^{[1
]}

张玲金 ^{[1
]}

李重九 ^{[2
]}

机构：

[1] 国家地质实验测试中心

[2] 中国农业大学

来源：

分析测试学报 | 2008年 / S1期

关键词：

polycyclic aromatic hydrocarbons(PAHs); accelerated solvent extraction(ASE); soil; GC-MS; residues analysis;

D O I：

暂无

中图分类号：

X833 [土壤监测];

学科分类号：

0903 ;

摘要：

In this study,a GC-MS/SIM method was used to analyze 16 PAHs in soil by ASE on-line clean-up.The average recoveries were ranged from 67% to 129%.The relative standard deviations were between 2.7% and 21.1%.The calculated limits of detection were no more than 0.95 ng/g.This method was fast,simple,and cost-saving,and can be used in the large quantities of samples analysis.

引用

页码：124 / 126+129 +129

页数：4

共 4 条

[1] 土壤样品中多环芳烃分析方法研究进展 [J].

平立凤 ;

李振 ;

赵华 ;

胡秀卿 ;

吴珉 .

土壤通报, 2007, (01) :179-184

[2] 加速溶剂萃取/气相色谱-质谱测定海洋沉积物中的痕量多环芳烃 [J].

李庆玲 ;

徐晓琴 ;

黎先春 ;

王小如 .

分析测试学报, 2006, (05) :33-37

[3] 微波萃取—高效液相色谱(HPLC)法测定土壤中16种多环芳烃的研究 [J].

杨杰 .

干旱环境监测, 2006, (01) :5-7

[4]

Extraction of polycyclic aromatic hydrocarbons and organochlorine pesticides from soils: A comparison between Soxhlet extraction, microwave-assisted extraction and accelerated solvent extraction techniques[J] . Wentao Wang,Bingjun Meng,Xiaoxia Lu,Yu Liu,Shu Tao.Analytica Chimica Acta . 2007 (2)

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