高速逆流色谱分离天然产物的溶剂体系选择

被引：59

作者：

张荣劲

杨义芳

机构：

[1] 上海医药工业研究院

来源：

中草药 | 2008年 / 02期

关键词：

HSCCC; 溶剂体系; 分离; 天然产物;

D O I：

暂无

中图分类号：

O657.72 [];

学科分类号：

摘要：

高速逆流色谱(HSCCC)是一种有效快速的分离方法。综述了近几年来关于HSCCC分离天然产物的研究进展,与以往综述按分离物质的种类对溶剂体系分类阐述不同,将按照溶剂体系的极性对其分类阐述,并且详细的论述了常用溶剂体系适合分离物质的特征,列举了大量的应用实例和被分离物质的结构及分配系数,对快速选择溶剂体系起到了一定的指导作用。最后介绍了一些新型的溶剂体系,对HSCCC的未来发展进行展望。

引用

页码：298 / 303

页数：6

共 41 条

[1]

基础结构化学.[M].张季爽，申成主编.科学出版社.2006,

[2]

微乳相萃取技术及应用.[M].刘会洲等著;.科学出版社.2005,

[3]

高速逆流色谱分离技术及应用.[M].曹学丽编著;.化学工业出版社.2005,

[4]

新型分离技术.[M].陈欢林主编;.化学工业出版社.2005,

[5]

化工分离工程.[M].邓修;吴俊生编著;.科学出版社.2000,

[6]

Preparative isolation and purification of two closely related glycosidic flavonoids from Exocarpium citri grandis by high-speed countercurrent chromatography [J].

Liang, Yong ;

Huang, Zhaofeng ;

Chen, Hongwei ;

Zhang, Tianyou ;

Ito, Yoichiro .

JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, 2007, 30 (03) :419-430

[7]

Two-step purification of scutellarin from Erigeron breviscapus (vant.) Hand. Mazz. by high-speed counter-current chromatography [J].

Gao, Min ;

Gu, Ming ;

Liu, Chun-zhao .

JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2006, 838 (02) :139-143

[8]

Optimization suitable conditions for preparative isolation and separation of curculigoside and curculigoside B from Curculigo orchioides by high-speed counter-current chromatography [J].

Peng, Jinyong ;

Jiang, Yunyun ;

Fan, Guorong ;

Chen, Bin ;

Zhang, Qiaoyan ;

Chai, Yifeng ;

Wu, Yutian .

SEPARATION AND PURIFICATION TECHNOLOGY, 2006, 52 (01) :22-28

[9]

Three-phase solvent systems for comprehensive separation of a wide variety of compounds by high-speed counter-current chromatography.[J].Yoichi Shibusawa;Yutaka Yamakawa;Ryoko Noji;Akio Yanagida;Heisaburo Shindo;Yoichiro Ito.Journal of Chromatography A.2006, 1

[10]

Isolation of hydroxycinnamoyltartaric acids from grape pomace by high-speed counter-current chromatography.[J].Thorsten Maier;Solveigh Sanzenbacher;Dietmar R. Kammerer;Nicolai Berardini;Jürgen Conrad;Uwe Beifuss;Reinhold Carle;Andreas Schieber.Journal of Chromatography A.2006, 1

← 1 2 3 4 5 →