在线凝胶色谱串联气相色谱-质谱对食品中七种杀菌剂残留量的测定

被引：13

作者：

杨惠琴

郭德华

李波

朱坚

盛永刚

董吉川

机构：

[1] 上海出入境检验检疫局

来源：

分析测试学报 | 2008年 / S1期

关键词：

GC-MS; bactericidal residues;

D O I：

暂无

中图分类号：

TS207.53 [];

学科分类号：

摘要：

The determination of 7 bactericidals residues,including chlorthalonil,dichlofluanid,tolylfluanid,captan,folpet,captafol and deltamethrin,in foods by using on-line gel permeation chromatography(GPC) coupled with gas chromatography-mass spectrometry(GC-MS).Bactericidal residues were extracted with acetonitrile,and cleaned up by ENVI-Crab,LC-NH2 column and GPC,respectively.The analysis of 7 bactericidals residues was performed by GC-MS.The average recoveries of analytes were range of 75%-120% with RSD of 3.5%-10.3%.

引用

页码：140 / 142

页数：3