4,4′-Bis(dimethylamino)benzhydryl phenyl sulfone

被引:3
作者
Baidya, Mahiuddin [1 ]
Mayr, Herbert [1 ]
Mayer, Peter [1 ]
机构
[1] Univ Munich, D-81377 Munich, Germany
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
GRAPH-SET ANALYSIS; CRYSTALS; PATTERNS; SCALES;
D O I
10.1107/S160053680904642X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C23H26N2O2S, the sulfur-bound phenyl group is aligned approximately parallel to one of the two rings of the benzhydryl group, making a dihedral angle of 1.15 (9)degrees. The other forms a dihedral angle of 59.20 (9)degrees with the phenyl group bound to the S atom. In the crystal, molecules are linked into strands along [100] by weak C-H center dot center dot center dot O contacts. Weak C-H center dot center dot center dot pi interactions are also observed.
引用
收藏
页码:O3035 / U98
页数:12
相关论文
共 18 条
[1]   SIR97:: a new tool for crystal structure determination and refinement [J].
Altomare, A ;
Burla, MC ;
Camalli, M ;
Cascarano, GL ;
Giacovazzo, C ;
Guagliardi, A ;
Moliterni, AGG ;
Polidori, G ;
Spagna, R .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 :115-119
[2]   PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].
BERNSTEIN, J ;
DAVIS, RE ;
SHIMONI, L ;
CHANG, NL .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573
[3]   GRAPH-SET ANALYSIS OF HYDROGEN-BOND PATTERNS IN ORGANIC-CRYSTALS [J].
ETTER, MC ;
MACDONALD, JC ;
BERNSTEIN, J .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1990, 46 :256-262
[4]  
Farrujia LJ., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]
[5]   The reaction between aromatic sulphinc acid and di- and triphenyl-carbinol. [J].
Hinsberg, O .
BERICHTE DER DEUTSCHEN CHEMISCHEN GESELLSCHAFT, 1917, 50 :468-473
[6]  
HINSBERG O, 1897, BER DTSCH CHEM GES, V30, P2803
[7]  
HOOFT RWW, 2004, COLLECT
[8]  
Kobayashi M., 1985, Sulfur Lett, V3, P117
[9]   4-methylphenyl benzyl sulfone [J].
Li, YS ;
Su, WK .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O2450-O2451
[10]  
Macrae CF, 2006, J APPL CRYSTALLOGR, V39, P453, DOI 10.1107/S0021 88980600731X