Detection of the chemical warfare agents bis-(2-chloroethyl)ethylamine (HN-1) and tris-(2-chloroethyl)amine (HN-3) in air

被引:22
作者
Stuff, JR
Cheicante, RL
Durst, HD
Ruth, JL
机构
[1] EAI Corp, Abingdon, MD 21009 USA
[2] Edgewood Res Dev & Engn Ctr, Aberdeen Proving Ground, MD 21010 USA
关键词
warfare agents; air analysis; method development; validation; chloroethylamines; amines; HN-1; HN-3;
D O I
10.1016/S0021-9673(99)00585-3
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
This paper describes the method development and validation for detection of the chemical warfare agents HN-1 and HN-3 in air using C-8 solid-phase extraction disks followed by Liquid desorption and analysis by gas chromatography. The method is contrasted to the standard approach which uses solid sorbent tubes followed by thermal desorption and analysis by gas chromatography. (C) 1999 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:529 / 540
页数:12
相关论文
共 14 条
[1]  
ELLZY MW, 1992, ERDECTR257
[2]   IDENTIFICATION OF CHEMICAL WARFARE AGENTS IN AIR SAMPLES USING CAPILLARY COLUMN GAS-CHROMATOGRAPHY WITH 3 SIMULTANEOUS DETECTORS [J].
KAIPAINEN, A ;
KOSTIAINEN, O ;
RIEKKOLA, ML .
JOURNAL OF MICROCOLUMN SEPARATIONS, 1992, 4 (03) :245-251
[3]  
KOOSTRA PR, 1995, J CHROMATOGR A, V697, P203
[4]  
KRIBBEN BD, 1983, TDMR735 EDG RES DEV
[5]  
LATTIN FG, 1996, P 1994 ERDEC SCI C C, P177
[6]   Fast determination of VOCs in workplace air by solid-phase extraction and gas chromatography - Mass spectrometry [J].
Mangani, F ;
Lattanzi, L ;
Maione, M .
CHROMATOGRAPHIA, 1998, 47 (1-2) :57-62
[7]  
MARKELL C, 1991, LC GC-MAG SEP SCI, V9, P332
[8]  
*MIN FOR AFF FINL, 1987, AIR MON MEANS VER CH
[9]  
MISKELLY PR, 1979, ARCSLTR80065 EDG RES
[10]  
National Research Council, 1993, ALT TECHN DESTR CHEM