Optimization of long-range 1H-15N 2D NMR experiments at natural abundance -: Assignment of the 15N resonances of cryptospirolepine at the submilligram level

被引：7

作者：

Hadden, CE ^{[1
]}

Martin, GE

Tackie, AN

Schiff, PL

机构：

[1] Pharmacia & Upjohn Inc, Rapid Struct Characterizat Grp, Pharmaceut Dev, Kalamazoo, MI 49001 USA

[2] Ctr Sci Res Plant Med, Mampong Akwapim, Ghana

[3] Univ Pittsburgh, Sch Pharm, Dept Pharmaceut Sci, Pittsburgh, PA 15261 USA

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 1999年 / 36卷 / 04期

关键词：

D O I：

10.1002/jhet.5570360449

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

引用

页码：1115 / 1117

页数：3

共 32 条

[1] H-1 AND C-13 ASSIGNMENTS FROM SENSITIVITY-ENHANCED DETECTION OF HETERONUCLEAR MULTIPLE-BOND CONNECTIVITY BY 2D MULTIPLE QUANTUM NMR [J].

BAX, A ;

SUMMERS, MF .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1986, 108 (08) :2093-2094

[2]

Bax A., 1982, 2 DIMENSIONAL NMR LI

[3] DIRECT DETERMINATION OF RATE CONSTANTS OF SLOW DYNAMIC PROCESSES BY TWO-DIMENSIONAL ACCORDION SPECTROSCOPY IN NUCLEAR MAGNETIC-RESONANCE [J].

BODENHAUSEN, G ;

ERNST, RR .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1982, 104 (05) :1304-1309

[4]

Brey W. S., 1988, PULSE METHODS 1D 2D

[5]

Croasmun W. R., 1994, 2 DIMENSIONAL NMR SP

[6] LONG-RANGE H-1-N-15 CORRELATION AT NATURAL-ABUNDANCE USING GRADIENT-ENHANCED INVERSE-DETECTION [J].

CROUCH, RC ;

MARTIN, GE .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 1995, 32 (05) :1665-1669

[7]

Ernst R. R., 1987, PRINCIPLES NUCL MAGN

[8]

Farley KA, 1997, MAGN RESON CHEM, V35, P671, DOI 10.1002/(SICI)1097-458X(199711)35:10<671::AID-OMR148>3.0.CO

[9]

2-0

[10] Low-level long-range 1H-15N heteronuclear shift correlation at natural abundance using submicro NMR techniques [J].

Hadden, CE ;

Martin, GE .

JOURNAL OF NATURAL PRODUCTS, 1998, 61 (08) :969-972

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