Solvothermal preparation of graphite-like C3N4 nanocrystals

被引：83

作者：

Bai, YJ

Lü, B

Liu, ZG

Li, L

Cui, DL

Xu, XG

Wang, QL

机构：

[1] Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Peoples R China

[2] Shandong Univ, Dept Mech Engn, Jinan 250031, Peoples R China

[3] Shandong Univ, Inst Chem & Chem Engn, Jinan 250100, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2003年 / 247卷 / 3-4期

基金：

中国国家自然科学基金; 中国博士后科学基金;

关键词：

transmission electron microscope; X-ray diffraction; nanomaterials; infrared devices;

D O I：

10.1016/S0022-0248(02)01981-4

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Graphite-like C3N4 nanocrystals were synthesized by the reaction Of CCl4 and NH4Cl at 400degreesC without any catalyst. XRD and TEM examinations indicate that the average size of the crystals is about 11 nm With a good crystallinity, and C = N and C-N bonds can be observed at 1617.95 and 1271.09 cm(-1) respectively, in the IR spectrum. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

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页码：505 / 508

页数：4

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