The contribution of phonon scattering to high-resolution images measured by off-axis electron holography

被引:27
作者
Boothroyd, CB
Dunin-Borkowski, RE
机构
[1] Inst Mat Res & Engn, Singapore 117602, Singapore
[2] Univ Cambridge, Dept Mat Sci & Met, Cambridge CB2 3QZ, England
关键词
phonon scattering; electron holography; high-resolution electron microscopy;
D O I
10.1016/j.ultramic.2003.08.005
中图分类号
TH742 [显微镜];
学科分类号
摘要
The contribution of electrons that have been phonon scattered to the lattice fringe amplitude and the background intensity of a high-resolution electron microscope (HREM) image is addressed experimentally through the analysis of a defocus series of energy-filtered off-axis electron holograms. It is shown that at a typical specimen thickness used for HREM imaging approximately 15% of the electrons that contribute to an energy-filtered image have been phonon scattered. At this specimen thickness, the phonon-scattered electrons contribute a lattice image of opposite contrast to the elastic lattice image. The overall lattice fringe contrast is then reduced to 70% of the value that it would have in the absence of phonon scattering. At higher specimen thickness, the behaviour is defocus-dependent, with the phonon image having lattice fringe contrast of either the same or the opposite sense to the elastic image as the defocus is varied. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:115 / 133
页数:19
相关论文
共 27 条
[1]   Quantification of high-resolution electron microscope images of amorphous carbon [J].
Boothroyd, CB .
ULTRAMICROSCOPY, 2000, 83 (3-4) :159-168
[2]   Why don't high-resolution simulations and images match? [J].
Boothroyd, CB .
JOURNAL OF MICROSCOPY, 1998, 190 :99-108
[3]  
Boothroyd CB, 1995, MATER RES SOC SYMP P, V354, P495
[4]   THE CONTRIBUTION OF INELASTICALLY SCATTERED ELECTRONS TO HIGH-RESOLUTION IMAGES OF (AL, GA)AS/GAAS HETEROSTRUCTURES [J].
BOOTHROYD, CB ;
STOBBS, WM .
ULTRAMICROSCOPY, 1988, 26 (04) :361-376
[5]   The phonon contribution to high-resolution electron microscope images [J].
Boothroyd, CB ;
Yeadon, M .
ULTRAMICROSCOPY, 2003, 96 (3-4) :361-365
[6]   THE CONTRIBUTION OF INELASTICALLY SCATTERED ELECTRONS TO HIGH-RESOLUTION [110] IMAGES OF ALAS/GAAS HETEROSTRUCTURES [J].
BOOTHROYD, CB ;
STOBBS, WM .
ULTRAMICROSCOPY, 1989, 31 (03) :259-274
[7]   ELECTRON-MICROSCOPY OF CRYSTALS WITH TIME-DEPENDENT PERTURBATIONS [J].
COWLEY, JM .
ACTA CRYSTALLOGRAPHICA SECTION A, 1988, 44 :847-853
[8]  
DERUIJTER WJ, 1994, MSA B, V24, P451
[9]  
DWYER C, 2003, IN PRESS ULTRAMICROS
[10]   QUANTITATIVE COMPARISON OF HIGH-RESOLUTION TEM IMAGES WITH IMAGE SIMULATIONS [J].
HYTCH, MJ ;
STOBBS, WM .
ULTRAMICROSCOPY, 1994, 53 (03) :191-203