Capillary electrophoretic determination of resveratrol in wines

被引:86
作者
Gu, XL
Creasy, L
Kester, A
Zeece, M [1 ]
机构
[1] Univ Nebraska, Dept Food Sci, Lincoln, NE 68583 USA
[2] Cornell Univ, Dept Fruit & Vegetable Sci, Ithaca, NY 14853 USA
关键词
resveratrol; wine; capillary electrophoresis;
D O I
10.1021/jf981211e
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
A rapid and sensitive capillary electrophoretic method for analysis of resveratrol in wine was established. The protocol consists of sample preparation using a C-18 solid-phase extraction cartridge. Baseline separation of trans- and cis-resveratrol from other compounds in wine was achieved in similar to 8 min using a micellar mode. The limits of detection for trans- and cis-resveratrol were 0.1 and 0.15 mu mol/L, respectively. Recovery rates for trans-resveratrol using the protocol described ranged from 94.6 +/- 8.5 to 101.9 +/- 7.2%. These procedures were used to analyze the trans- and cis-resveratrol levels in 26 wines. It was found that the concentration of trans-resveratrol ranged from 0.987 to 25.4 mu mol/L, whereas the concentration of cis-resveratrol was much lower.
引用
收藏
页码:3223 / 3227
页数:5
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