A room-temperature synthesis of nanocrystalline vanadium nitride

被引：29

作者：

Chen, LY

Gu, YL

Shi, L

Yang, ZH

Ma, JH

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

来源：

SOLID STATE COMMUNICATIONS | 2004年 / 132卷 / 05期

关键词：

vanadium nitride; chemical synthesis; transmission electron microscopy; X-ray diffraction;

D O I：

10.1016/j.ssc.2004.07.041

中图分类号：

O469 [凝聚态物理学];

学科分类号：

070205 ;

摘要：

Vanadium nitride was synthesized by the reaction Of VCl4 and NaNH2 at room temperature. X-ray powder diffraction could be indexed as cubic VN with the lattice constant of a = 4.134 Angstrom. Transmission electron microscopy image showed particle and hollow sphere morphology. The optical properties of the as-prepared VN were investigated. (C) 2004 Published by Elsevier Ltd.

引用

页码：343 / 346

页数：4

共 16 条

[1] Dean J., 1979, LANGES HDB CHEM
[2] Ternary nitrides: A rapidly growing class of new materials
DiSalvo, FJ
Clarke, SJ
[J]. CURRENT OPINION IN SOLID STATE & MATERIALS SCIENCE, 1996, 1 (02) : 241 - 249
[3] PRAPARATION UND SUPRALEITUNGSEIGENSCHAFTEN VON REINEM SOWIE ZIRKON- UND TITANHALTIGEM NIOBNITRID
HECHLER, K
SAUR, E
[J]. ZEITSCHRIFT FUR PHYSIK, 1967, 205 (04): : 392 - &
[4] Solid state metathesis reaction for metal borides, silicides, pnictides and chalcogenides: Ionic or elemental pathways
Parkin, IP
[J]. CHEMICAL SOCIETY REVIEWS, 1996, 25 (03) : 199 - +
[5] Atmospheric pressure chemical vapour deposition of vanadium nitride and oxynitride films on glass from reaction of VCl4 with NH3
Parkin, IP
Elwin, GS
[J]. JOURNAL OF MATERIALS CHEMISTRY, 2001, 11 (12) : 3120 - 3124
[6] A STUDY OF SUPERCONDUCTIVITY IN INTERSTITIAL COMPOUNDS
PESSALL, N
GOLD, RE
JOHANSEN, HA
[J]. JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1968, 29 (01) : 19 - &
[7] PREPARATION AND SUPERCONDUCTING PROPERTIES OF ULTRAFINE POWDERS AND SINTERED COMPACTS OF NBC AND NBN
POWELL, RM
SKOCPOL, WJ
TINKHAM, M
[J]. JOURNAL OF APPLIED PHYSICS, 1977, 48 (02) : 788 - 794
[8] ROMAND M, 1976, ANALUSIS, V4, P308
[9] ELECTRON-ENERGY-LOSS-SPECTROSCOPY AND ULTRAVIOLET-PHOTOEMISSION-SPECTROSCOPY STUDY OF THE VNX SYSTEM
SCHUBERT, WK
SHELTON, RN
WOLF, EL
[J]. PHYSICAL REVIEW B, 1981, 23 (10): : 5097 - 5106
[10] Shaffer P. T. B, 1964, PLENUM PRESS HDB HIG

← 1 2 →