A multiresidue method for the determination of insecticides and triazine herbicides in fresh and processed olives

被引:18
作者
Avramides, Elizabeth J.
Gkatsos, Sotiris
机构
[1] Natl Agr Res Fdn, NAGREF, Athens 14123, Greece
[2] Natl Tech Univ Athens, Sch Chem Engn, GR-15773 Athens, Greece
关键词
olives; organophosphorus insecticides; pyrethroid insecticides; triazines; residues;
D O I
10.1021/jf062826b
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
A simple, rapid, and low-cost gas chromatographic multiresidue method has been developed for the analysis of pesticide residues in raw and processed olives. This has been validated for 19 insecticides and triazine herbicides, covering a wide range of polarities. The method uses low-temperature precipitation to remove lipids and gives good cleanup for gas chromatography analysis with nitrogen phosphorus and electron capture detection. Recoveries are between 71 and 99%, with relative standard deviation values of 5-15%.
引用
收藏
页码:561 / 565
页数:5
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