Microwave hydrothermal synthesis of nanocrystalline rutile

被引：25

作者：

Chen, Zhiqin ^{[1
,2
]}

Li, Wenkui ^{[1
,2
]}

Zeng, Weijun ^{[3
]}

Li, Mingsheng ^{[1
,2
]}

Xiang, Junhuai ^{[1
,2
]}

Zho, Zehua ^{[1
,2
]}

Huang, Junlin ^{[2
]}

机构：

[1] Jiangxi Sci & Technol Normal Univ, Jiangxi Key Lab Surface Engn, Nanchang 330013, Peoples R China

[2] Jiangxi Sci & Technol Normal Univ, Sch Mat Sci & Engn, Nanchang 330013, Peoples R China

[3] Jiangxi Acad Sci, Inst Appl Phys, Nanchang 330029, Peoples R China

来源：

MATERIALS LETTERS | 2008年 / 62卷 / 28期

关键词：

ceramic; rutile; microwave hydrothermal method; nanomaterials;

D O I：

10.1016/j.matlet.2008.07.024

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Titanium dioxide of the rutile phase has been synthesized using titanium tetrachloride and hydrochloric acid by means of microwave hydrothermal method. The mixture solution is processed in microwave hydrothermal autoclave first at 120 degrees C for 1.5 h and then at 180 degrees C for 1 h to precipitate rutile powders. it was revealed that well-dispersed and shuttle-like rutile TiO2 with the average diameter of 10 nm was formed by means of XRD and TEM. (C) 2008 Elsevier B.V. All rights reserved.

引用

页码：4343 / 4344

页数：2

共 18 条

[1]

AMBRUS Z, 2008, APPL CATAL B-ENVIRON, V81, P32

[2] Microwave-hydrothermal process for the synthesis of rutile [J].

Baldassari, S ;

Komarneni, S ;

Mariani, E ;

Villa, C .

MATERIALS RESEARCH BULLETIN, 2005, 40 (11) :2014-2020

[3] HYDROTHERMAL PREPARATION OF UNIFORM NANOSIZE RUTILE AND ANATASE PARTICLES [J].

CHENG, HM ;

MA, JM ;

ZHAO, ZG ;

QI, LM .

CHEMISTRY OF MATERIALS, 1995, 7 (04) :663-671

[4] Shape-controlled synthesis of nanocrystalline titania at low temperature [J].

Chu, RH ;

Yan, JC ;

Lian, SY ;

Wang, YH ;

Yan, FC ;

Chen, DW .

SOLID STATE COMMUNICATIONS, 2004, 130 (12) :789-792

[5] Synthesis of nanocrystalline TiO2 at 100 °C [J].

Dhage, SR ;

Choube, VD ;

Samuel, V ;

Ravi, V .

MATERIALS LETTERS, 2004, 58 (17-18) :2310-2313

[6] Synthesis of ultrafine TiO2 by citrate gel method [J].

Dhage, SR ;

Pasricha, R ;

Ravi, V .

MATERIALS RESEARCH BULLETIN, 2003, 38 (11-12) :1623-1628

[7]

HUMIN C, 1995, CHEM MATER, V7, P667

[8] Homogeneous precipitation of TiO2 ultrafine powders from aqueous TiOCl2 solution [J].

Kim, SJ ;

Park, SD ;

Jeong, YH ;

Park, S .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1999, 82 (04) :927-932

[9] Microwave-hydrothermal processing of titanium dioxide [J].

Komarneni, S ;

Rajha, RK ;

Katsuki, H .

MATERIALS CHEMISTRY AND PHYSICS, 1999, 61 (01) :50-54

[10] SYNTHESIS AND TEXTURAL PROPERTIES OF UNSUPPORTED AND SUPPORTED RUTILE (TIO2) MEMBRANES [J].

KUMAR, KNP ;

KEIZER, K ;

BURGGRAAF, AJ ;

OKUBO, T ;

NAGAMOTO, H .

JOURNAL OF MATERIALS CHEMISTRY, 1993, 3 (09) :923-929

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