MgFe2O4 pigment obtained at low temperature

被引:64
作者
Candeia, RA
Souza, MAF
Bernardi, MIB
Maestrelli, SC
Santos, IMG
Souza, AG
Longo, E
机构
[1] UFPB, LTM, Dept Chem, CCEN, BR-58059900 Joao Pessoa, Paraiba, Brazil
[2] USP, Crystal Growth & Ceram Mat Grp, CMDMC, Dept Phys & Mat Sci,Inst Phys Sao Carlos, BR-13560970 Sao Carlos, SP, Brazil
[3] UFSCar, CMDMC, Dept Chem, CCT, BR-13565905 Sao Carlos, SP, Brazil
[4] UFSCar, Dept Mat Engn, BR-13565905 Sao Carlos, SP, Brazil
基金
巴西圣保罗研究基金会;
关键词
ceramics; inorganic compounds; chemical synthesis; X-ray diffraction;
D O I
10.1016/j.materresbull.2005.07.019
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
This work had the objective of studying the pigment MgFe2O4 obtained by the polymeric precursor method, which is based on the formation of a polymeric resin, followed by a heat treatment in order to obtain the final oxide. The powders were calcined between 500 and 1100 degrees C, and characterized by thermal analysis, X-ray diffraction, nitrogen adsorption, scanning electronic microscopy and diffuse reflectance. The pigment is single phase, with a cubic system and space group Fd3m (2 2 7). A low temperature synthesis was possible, with a crystalline material after heat treatment at 800 degrees C. The colors obtained varied, according to the crystallization of the MgFe2O4. (C) 2005 Elsevier Ltd. All rights reserved.
引用
收藏
页码:183 / 190
页数:8
相关论文
共 24 条
[1]   Synthesis and characterization of spinel pigment CaFe2O4 obtained by the polymeric precursor method [J].
Candeia, RA ;
Bernardi, MIB ;
Longo, E ;
Santos, IMG ;
Souza, AG .
MATERIALS LETTERS, 2004, 58 (05) :569-572
[2]   Crystallization of ceramic pigment CoAl2O4 nanocrystals from Co-Al metal organic precursor [J].
Cho, WS ;
Kakihana, M .
JOURNAL OF ALLOYS AND COMPOUNDS, 1999, 287 (1-2) :87-90
[3]  
CULLITY BD, 1956, ELEMENTS XRAY DIFFRA, V9, P259
[4]  
Ettre L. S., 1987, PIGMENT HDB, P139
[5]  
Ezhilvalavan S, 1996, APPL PHYS LETT, V68, P2693, DOI 10.1063/1.116311
[6]   Thermal study of CoxZn7-xSb2O12 spinel obtained by Pechini method using different alcohols [J].
Gouveia, DS ;
Rosenhaim, R ;
de Maurera, MAMA ;
Lima, SJG ;
Paskocinas, CA ;
Longo, E ;
Souza, AG ;
Santos, IMG .
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2004, 75 (02) :453-460
[7]   Preparation, structure and electrochemical properties of spinel Li1-xMn2-yO4 cathode material for lithium ion batteries [J].
Huang, KL ;
Peng, B ;
Chen, ZH ;
Huang, PY .
SOLAR ENERGY MATERIALS AND SOLAR CELLS, 2000, 62 (1-2) :177-185
[8]   Polymerized complex route to the synthesis of pure SrTiO3 at reduced temperatures:: Implication for formation of Sr-Ti heterometallic citric acid complex [J].
Kakihana, M ;
Okubo, T ;
Arima, M ;
Nakamura, Y ;
Yashima, M ;
Yoshimura, M .
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 1998, 12 (02) :95-109
[9]   ''Sol-Gel'' preparation of high temperature superconducting oxides [J].
Kakihana, M .
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 1996, 6 (01) :7-55
[10]   IR spectroscopic investigation of cation distribution in Zn-Co oxide catalysts with spinel type structure [J].
Kustova, GN ;
Burgina, EB ;
Volkova, GG ;
Yurieva, TM ;
Plyasova, LM .
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2000, 158 (01) :293-296