Resolution of cis-4-O-TBS-2-cyclopenten-1,4-diol

被引：21

作者：

Curran, TT

Hay, DA

机构：

[1] Hoechst Marion Roussel Pharmaceut., Cincinnati, OH 45215

[2] Wyeth-Ayerst Research, Bldg. 222, Pearl River, NY 10965

来源：

TETRAHEDRON-ASYMMETRY | 1996年 / 7卷 / 10期

关键词：

D O I：

10.1016/0957-4166(96)00363-1

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The resolution of cis-4-O-TBS-2-cyclopenten-1,4-diol with a few different enzymes in organic medium is described. The optical purity and yield of both the alcohol and acetate were moderate to excellent. Copyright (C) 1996 Elsevier Science Ltd

引用

页码：2791 / 2792

页数：2

共 15 条

[1] SYNTHESIS OF CHIRAL CARBOCYCLIC NUCLEOSIDES [J].

BORTHWICK, AD ;

BIGGADIKE, K .

TETRAHEDRON, 1992, 48 (04) :571-623

[2] SYNTHESIS OF THERAPEUTICALLY USEFUL PROSTAGLANDIN AND PROSTACYCLIN ANALOGS [J].

COLLINS, PW ;

DJURIC, SW .

CHEMICAL REVIEWS, 1993, 93 (04) :1533-1564

[3]

DEARDORFF DR, 1995, ORG SYNTH, V73, P25

[4] SYNTHESIS OF THE 4 POSSIBLE STEREOISOMERIC 5'-NOR CARBOCYCLIC NUCLEOSIDES FROM ONE COMMON ENANTIOMERICALLY PURE STARTING MATERIAL [J].

DYATKINA, N ;

COSTISELLA, B ;

THEIL, F ;

VONJANTALIPINSKI, M .

TETRAHEDRON LETTERS, 1994, 35 (13) :1961-1964

[5] ENZYMATIC ASYMMETRIZATION OF MESO-2-CYCLOALKEN-1,4-DIOLS AND THEIR DIACETATES IN ORGANIC AND AQUEOUS-MEDIA [J].

JOHNSON, CR ;

BIS, SJ .

TETRAHEDRON LETTERS, 1992, 33 (48) :7287-7290

[6] ENZYMATIC-HYDROLYSIS OF PROCHIRAL CIS-1,4-DIACYL-2-CYCLOPENTENEDIOLS - PREPARATION OF (1S,4R) AND (1R,4S)-4-HYDROXY-2-CYCLOPENTENYLDERIVATIVES, VERSATILE BUILDING-BLOCKS FOR CYCLOPENTANOID NATURAL-PRODUCTS [J].

LAUMEN, K ;

SCHNEIDER, M .

TETRAHEDRON LETTERS, 1984, 25 (51) :5875-5878

[7] An improved preparation of highly enantiomerically enriched (R)-(+)-4-tert-butyldimethylsiloxy-2-cyclopenten-1-one [J].

Myers, AG ;

Hammond, M ;

Wu, YS .

TETRAHEDRON LETTERS, 1996, 37 (18) :3083-3086

[8]

Paquett LA., 1995, ORG SYNTH, V73, P36

[9]

PAQUETTE LA, 1995, ORG SYNTH, V73, P44

[10] Enantioselective synthesis through enzymatic asymmetrization [J].

Schoffers, E ;

Golebiowski, A ;

Johnson, CR .

TETRAHEDRON, 1996, 52 (11) :3769-3826

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