Synthesis and characterization of lanthanum carbide nanotubes

被引:3
作者
Awasthi, K [1 ]
Singh, AK [1 ]
Srivastava, ON [1 ]
机构
[1] Banaras Hindu Univ, Dept Phys, Varanasi 221005, Uttar Pradesh, India
关键词
lanthanum carbide nanotubes; nanorods; arc evaporation; transmission electron microscopy; X-ray diffractometry; lanthanum carbide;
D O I
10.1166/jnn.2002.078
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Lanthanum carbide nanotubes have been synthesized by d.c. arc evaporation (similar to20-30 V, similar to200 Amp) of lanthanum metal (90 wt.%)-loaded graphite rod in a helium atmosphere (665 mbar). To explore the possibility of formation of lanthanum carbide nanotubes, the experiments were carried out with lanthanum metal in different concentrations (i.e., 30, 50, 70, and 90 wt.%) in the graphite rod. The as-synthesized samples were characterized by transmission electron microscopy and X-ray diffractometry. Lanthanum carbide nanotubes (LCNTs) with a diameter of similar to65 to 95 nm and a length of similar to0.2 to 1.5 mum were obtained in this study.
引用
收藏
页码:67 / 71
页数:5
相关论文
共 27 条
[1]   CAPILLARITY-INDUCED FILLING OF CARBON NANOTUBES [J].
AJAYAN, PM ;
IIJIMA, S .
NATURE, 1993, 361 (6410) :333-334
[2]   Synthesis of carbon nanotubes through carbon arc evaporation employing Mm, La, and Ce catalysts [J].
Awasthi, K ;
Singh, AK ;
Srivastava, ON .
FULLERENE SCIENCE AND TECHNOLOGY, 2001, 9 (03) :397-407
[3]   SYNTHESIS AND CHARACTERIZATION OF CARBIDE NANORODS [J].
DAI, HJ ;
WONG, EW ;
LU, YZ ;
FAN, SS ;
LIEBER, CM .
NATURE, 1995, 375 (6534) :769-772
[4]   CAPILLARITY AND WETTING OF CARBON NANOTUBES [J].
DUJARDIN, E ;
EBBESEN, TW ;
HIURA, H ;
TANIGAKI, K .
SCIENCE, 1994, 265 (5180) :1850-1852
[5]   HIGH-RATE, GAS-PHASE GROWTH OF MOS2 NESTED INORGANIC FULLERENES AND NANOTUBES [J].
FELDMAN, Y ;
WASSERMAN, E ;
SROLOVITZ, DJ ;
TENNE, R .
SCIENCE, 1995, 267 (5195) :222-225
[6]   Cage structures and nanotubes of NiCl2 [J].
Hacohen, YR ;
Grunbaum, E ;
Tenne, R ;
Sloan, J ;
Hutchison, JL .
NATURE, 1998, 395 (6700) :336-337
[7]  
Harris G.L., 1995, Properties of Silicon Carbide
[8]   Electrochemical formation of novel nanowires and their dynamic effects [J].
Hsu, WK ;
Terrones, M ;
Terrones, H ;
Grobert, N ;
Kirkland, AI ;
Hare, JP ;
Prassides, K ;
Townsend, PD ;
Kroto, HW ;
Walton, DRM .
CHEMICAL PHYSICS LETTERS, 1998, 284 (3-4) :177-183
[9]   HELICAL MICROTUBULES OF GRAPHITIC CARBON [J].
IIJIMA, S .
NATURE, 1991, 354 (6348) :56-58
[10]   ENCAPSULATION OF LANTHANUM CARBIDE IN CARBON NANOTUBES AND CARBON NANOPARTICLES [J].
LIU, MQ ;
COWLEY, JM .
CARBON, 1995, 33 (02) :225-232