Surface energy and surface area measurements by 19F MAS NMR of adsorbed trifluoroacetic acid

被引：11

作者：

Budarin, VL ^{[1
]}

Clark, JH ^{[1
]}

Tavener, SJ ^{[1
]}

机构：

[1] Univ York, Dept Chem, York YO10 5DD, N Yorkshire, England

来源：

CHEMICAL COMMUNICATIONS | 2004年 / 05期

关键词：

D O I：

10.1039/b315005d

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Trifluoroacetic acid, when adsorbed on the surface of inorganic materials, is a useful F-19 NMR probe molecule for studying surface properties including surface energy and surface area.

引用

页码：524 / 525

页数：2

共 15 条

[1] Correlation between volume and surface adsorption. Adsorption on nanoparticles [J].

Dobruskin, VK .

LANGMUIR, 2003, 19 (06) :2134-2146

[2]

Dubinin M. M., 1947, DOKL AKAD NAUK SSSR, V55, P331

[3] 19F MAS NMR quantification of accessible hydroxyl sites on fiberglass surfaces [J].

Fry, RA ;

Tsomaia, N ;

Pantano, CG ;

Mueller, KT .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2003, 125 (09) :2378-2379

[4]

Günther H, 1999, MAGN RESON CHEM, V37, pS142, DOI 10.1002/(SICI)1097-458X(199912)37:13<S142::AID-MRC573>3.0.CO

[5]

2-1

[6] NMR characterization of Bronsted acid sites in faujasitic zeolites with use of perdeuterated trimethylphosphine oxide [J].

Karra, MD ;

Sutovich, KJ ;

Mueller, KT .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2002, 124 (06) :902-903

[7] On the applicability of the classical dipole-dipole interaction for polar Bose-Einstein condensates [J].

Konotop, VV ;

Pérez-García, VM .

PHYSICS LETTERS A, 2002, 300 (4-5) :348-352

[8] Determination of the specific surface area and the pore size of microporous carbons from adsorption potential distributions [J].

Kruk, M ;

Jaroniec, M ;

Gadkaree, KP .

LANGMUIR, 1999, 15 (04) :1442-1448

[9] The use of Reichardt's dye as an indicator of surface polarity [J].

Macquarrie, DJ ;

Tavener, SJ ;

Gray, GW ;

Heath, PA ;

Rafelt, JS ;

Saulzet, SI ;

Hardy, JJE ;

Clark, JH ;

Sutra, P ;

Brunel, D ;

di Renzo, F ;

Fajula, F .

NEW JOURNAL OF CHEMISTRY, 1999, 23 (07) :725-731

[10] Measurement of the global acidity of solid acids by 31P MAS NMR of chemisorbed triethylphosphine oxide [J].

Osegovic, JP ;

Drago, RS .

JOURNAL OF PHYSICAL CHEMISTRY B, 2000, 104 (01) :147-154

← 1 2 →