Low Solvothermal Synthesis and Characterization of Hollow Nanospheres Molybdenum Sulfide

被引：21

作者：

Akram, H. ^{[1
,2
]}

Mateos-Pedrero, C. ^{[1
]}

Gallegos-Suarez, E. ^{[1
]}

Allali, N. ^{[2
]}

Chafik, T. ^{[2
]}

Rodriguez-Ramos, I. ^{[1
]}

Guerrero Ruiz, A. ^{[1
]}

机构：

[1] UA UNED ICP CSIC, Inst Catalisis & Petroleoquim, Grp Diseno Mol Catalizadores Heterogeneos, Madrid 28049, Spain

[2] Univ Abdelmalek Essaadi, Fac Sci & Tech Tanger, Lab Genie Chim & Valorisat Ressources, Tangier, Morocco

来源：

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY | 2012年 / 12卷 / 08期

关键词：

Molybdenum Disulfide; Solvothermal Synthesis; Hollow Nanospheres; HIGH-SURFACE-AREA; NANOCRYSTALLINE MOS2; DISULFIDE; ROUTE; MOO3;

D O I：

10.1166/jnn.2012.4561

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Hollow nanospheres of molybdenum disulfide have been synthesized by a novel solvothermal method under low temperature (180 degrees C). These nanomaterials were characterized by X-ray diffraction (XRD), Fourier transformation infra-red spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM, HRTEM) and X-ray Photoelectron Spectroscopy (XPS). A mechanism for the synthesis reaction is tentatively proposed and discussed.

引用

页码：6679 / 6685

页数：7

共 19 条

[1] Genesis of vesicle-like and tubular morphologies in inorganic precipitates: Amorphous Mo oxysulfides [J].