Coupling NMR to NOM

被引：80

作者：

Cook, RL

机构：

[1] Louisiana State Univ, Dept Chem, Baton Rouge, LA 70803 USA

[2] Southern Univ, Baton Rouge, LA 70803 USA

来源：

ANALYTICAL AND BIOANALYTICAL CHEMISTRY | 2004年 / 378卷 / 06期

关键词：

natural organic matter; humic acid; fulvic acid; solid state; liquid state; multi-dimensional; nuclear magnetic resonance;

D O I：

10.1007/s00216-003-2422-z

中图分类号：

Q5 [生物化学];

学科分类号：

071010 [生物化学与分子生物学]; 081704 [应用化学];

摘要：

This work itemizes and critically assesses several 1 D and multi-dimensional nuclear magnetic resonance (NMR) techniques, in both the liquid (solvent suppression, APT, DEPT, INEPT, COSY, TOCSY, HSQC, HMQC, HMBC, NOESY, ROESY and others) and solid states (DP, SACP, RAMP-CP, CP-TOSS, MQ-DEPT, 2D H-1-C-13 HETCOR and others), which are relevant to the characterization of natural organic matter (NOM). The pros and cons of many of the discussed techniques are compared in an effort to provide guidance to the most beneficial utilization of these NMR instrumental techniques for researchers interested in gaining insight into various aspects of NOM.

引用

页码：1484 / 1503

页数：20

共 111 条

[1]

Elucidation of aluminum-fulvic acid interactions by gas-phase hydrogen/deuterium (H/D) exchange and electrospray Fourier transform ion cyclotron resonance mass spectrometry (ESI FT-ICR) [J].