Measurement of magnetic susceptibility and calculation of shape factor of NMR samples

被引：57

作者：

Hoffman, RE ^{[1
]}

机构：

[1] Hebrew Univ Jerusalem, Dept Organ Chem, IL-91904 Jerusalem, Israel

来源：

JOURNAL OF MAGNETIC RESONANCE | 2006年 / 178卷 / 02期

关键词：

shape factor; susceptibility; chemical shift; BMS shift;

D O I：

10.1016/j.jmr.2005.09.009

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A method for accurate measurement of magnetic susceptibility and determination of the shape factor in ail NMR tube is shown. The combination of accurate shape factor determination with susceptibility measurement leads to improved accuracy when measuring chemical shift. This is important for comparing samples in different solvents or under different conditions, such as temperature, solvent, and pH. (c) 2005 Elsevier Inc. All rights reserved.

引用

页码：237 / 247

页数：11

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