Redetermination of L-leucine at 120 K

被引：58

作者：

Gorbitz, CH

Dalhus, B

机构：

[1] Department of Chemistry, University of Oslo, N-0315 Oslo

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1996年 / 52卷 / Pt 7期

关键词：

D O I：

10.1107/S0108270196002296

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

This redetermination of L-leucine, C6H13NO2, forms part III in a series of crystal structure determinations of hydrophobic amino acids. The L-leucine crystals were grown from a dilute acetic acid solution, E.s.d.'s for bond lengths between heavy atoms are in the range 0.001-0.002 Angstrom.

引用

页码：1754 / 1756

页数：3

共 8 条

[1] SIR92 - a program for automatic solution of crystal structures by direct methods [J].

ALTOMARE, A ;

CASCARANO, G ;

GIACOVAZZO, G ;

GUAGLIARDI, A ;

BURLA, MC ;

POLIDORI, G ;

CAMALLI, M .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1994, 27 :435-435

[2] STRUCTURE OF L-LEUCINE - A REDETERMINATION [J].

COLL, M ;

SOLANS, X ;

FONTALTABA, M ;

SUBIRANA, JA .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1986, 42 :599-601

[3]

DALHUS B, 1996, IN PRESS ACTA CHEM S, V50

[4] L-isoleucine, redetermination at 120 K [J].

Gorbitz, CH ;

Dalhus, B .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 (06) :1464-1466

[5] L-LEUCINE [J].

HARDING, MM ;

HOWIESON, RM .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1976, 32 (FEB15) :633-634

[6]

Johnson C. K., 1976, ORNL5138

[7]

SHELDRICK GM, 1993, SHELXL93 PROGRAM REF

[8] COMPARISON OF X-RAY AND NEUTRON-DIFFRACTION RESULTS FOR THE N-H...O=C HYDROGEN-BOND [J].

TAYLOR, R ;

KENNARD, O .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1983, 39 (FEB) :133-138

← 1 →