Chemical characterization of in vivo aged zinc phosphate dental cements

被引:23
作者
Margerit, J [1 ]
Cluzel, B [1 ]
Leloup, JM [1 ]
Nurit, J [1 ]
Pauvert, B [1 ]
Terol, A [1 ]
机构
[1] FAC PHARM MONTPELLIER,LAB CHIM GEN & MINERALE,MONTPELLIER,FRANCE
关键词
D O I
10.1007/BF00058202
中图分类号
R318 [生物医学工程];
学科分类号
0831 [生物医学工程];
摘要
The chemical composition of zinc phosphate dental cements aged in vivo was studied. Twenty-seven samples aged 2 to 43 years were investigated using X-ray diffraction, infrared spectroscopy, P-31 nuclear magnetic resonance spectroscopy, thermogravimetric analysis and differential scanning calorimetry. Evidence for the presence of zinc oxide, amorphous zinc phosphate, water of hydration and crystalline zinc phosphate tetrahydrate was found. The latter was identified as hopeite; it was present in 92% of the cements studied. No correlation with time concerning either the chemical structure of the components or their relative amounts was found. Zinc phosphate dental cements show very good chemical stability on long-term use.
引用
收藏
页码:623 / 628
页数:6
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