Trends in solid-phase microextraction for determining organic pollutants in environmental samples

被引：152

作者：

Peñalver, A ^{[1
]}

Pocurull, E ^{[1
]}

Borrull, F ^{[1
]}

Marcé, RM ^{[1
]}

机构：

[1] Univ Rovira & Virgili, Dept Quim Analit & Quim Organ, Tarragona 43005, Spain

来源：

TRAC-TRENDS IN ANALYTICAL CHEMISTRY | 1999年 / 18卷 / 08期

关键词：

solid-phase microextraction; environmental analysis; organic compounds; extraction techniques;

D O I：

10.1016/S0165-9936(99)00145-4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Solid-phase microextraction (SPME) is a recent technique for sample preparation, It has been used successfully to analyze environmental pollutants in a variety of matrices such as soils, water, and air. SPME is a solvent-free technique which has a number of advantages over more conventional sample preparation techniques such as liquid-liquid extraction (LLE) and solid-phase extraction (SPE), We describe the most recent developments in SPME and some which are being developed, including its coupling to HPLC and CE, the use of new fibers, and the automation of the entire SPME process and its application to field analysis. A summary is given of the most important parameters for applying this extraction technique to the analysis of environmental samples. (C) 1999 Elsevier Science B,V, All rights reserved.

引用

页码：557 / 568

页数：12

共 50 条

[31]

NILSSON T, 1995, HRC-J HIGH RES CHROM, V18, P617

[32] Application of solid-phase microextraction to the headspace gas chromatographic analysis of semi-volatile organochlorine contaminants in aqueous matrices [J].

Page, BD ;

Lacroix, G .

JOURNAL OF CHROMATOGRAPHY A, 1997, 757 (1-2) :173-182

[33] Derivatization/solid-phase microextraction: New approach to polar analytes [J].

Pan, L ;

Pawliszyn, J .

ANALYTICAL CHEMISTRY, 1997, 69 (02) :196-205

[34] DETERMINATION OF FATTY-ACIDS USING SOLID-PHASE MICROEXTRACTION [J].

PAN, L ;

ADAMS, M ;

PAWLISZYN, J .

ANALYTICAL CHEMISTRY, 1995, 67 (23) :4396-4403

[35] Water solubility and octanol/water-partitioning of hydrophobic chlorinated organic substances determined by using SPME/GC [J].

Paschke, A ;

Popp, P ;

Schuurmann, G .

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1998, 360 (01) :52-57

[36]

Pawliszyn J., 1997, SOLID PHASE MICROEXT

[37] Solid phase microextraction of volatile organic compounds using carboxen-polydimethylsiloxane fibers [J].

Popp, P ;

Paschke, A .

CHROMATOGRAPHIA, 1997, 46 (7-8) :419-424

[38] Solid-phase microextraction for determining the binding state of organic pollutants in contaminated water rich in humic organic matter [J].

Pörschmann, J ;

Kopinke, FD ;

Pawliszyn, J .

JOURNAL OF CHROMATOGRAPHY A, 1998, 816 (02) :159-167

[39] Solid-phase microextraction [J].

Prosen, H ;

Zupancic-Kralj, L .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 1999, 18 (04) :272-282

[40] Analysis of chlorobenzenes in soils by headspace solid-phase microextraction and gas chromatography ion trap mass spectrometry [J].

Santos, FJ ;

Sarrion, MN ;

Galceran, MT .

JOURNAL OF CHROMATOGRAPHY A, 1997, 771 (1-2) :181-189

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