Synthesis of exfoliated graphite from fluorinated graphite using an atmospheric-pressure argon plasma

被引：29

作者：

Manning, TJ ^{[1
]}

Mitchell, M

Stach, J

Vickers, T

机构：

[1] Valdosta State Univ, Dept Chem, Valdosta, GA 31698 USA

[2] Adv Energy, Voorhees, NJ USA

[3] Florida State Univ, Dept Chem, Tallahassee, FL 32306 USA

来源：

CARBON | 1999年 / 37卷 / 07期

关键词：

exfoliated graphite; intercalation compounds; Raman spectroscopy; SEM;

D O I：

10.1016/S0008-6223(98)00316-9

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Synthesis of a stable form of exfoliated graphite (EG) is described. EG was prepared from the Graphite Intercalation Compound (GIC) fluorine-graphite using an atmospheric-pressure 27.12 MHz inductively coupled argon plasma. The fluorinated graphite dust is continuously injected into the argon plasma (5000-8000 K), and collected. Raman spectroscopy and scanning electron microscopy (SEM) images are used to identify nanotubular structures at the terminals of the EG graphite sheets. (C) 1999 Elsevier Science Ltd. All rights reserved.

引用

页码：1159 / 1164

页数：6

共 41 条

[1] EXFOLIATION OF INTERCALATED GRAPHITE [J].

ANDERSON, SH ;

CHUNG, DDL .

CARBON, 1984, 22 (03) :253-263

[2] PHYSICAL-PROPERTIES OF DENSE EXPANDED GRAPHITE [J].

BERGER, D ;

MAIRE, J .

MATERIALS SCIENCE AND ENGINEERING, 1977, 31 :335-339

[3] STRUCTURE AND VIBRATIONAL PROPERTIES OF CARBON TUBULES [J].

CHANDRABHAS, N ;

SOOD, AK ;

SUNDARARAMAN, D ;

RAJU, S ;

RAGHUNATHAN, VS ;

RAO, GVN ;

SASTRY, VS ;

RADHAKRISHNAN, TSR ;

HARIHARAN, Y ;

BHARATHI, A ;

SUNDAR, CS .

PRAMANA-JOURNAL OF PHYSICS, 1994, 42 (05) :375-385

[4]

COOK J, 1996, CHEM IND, V19, P600

[5]

DOWELL MB, 1975, 12 BIENN C CARB PITT, P31

[6]

Dresselhaus M, 1996, PHYS WORLD, V9, P18

[7]

Dresselhaus M. S., 1996, SCI FULLERENES CARBO

[8] INTERCALATION COMPOUNDS OF GRAPHITE [J].

DRESSELHAUS, MS ;

DRESSELHAUS, G .

ADVANCES IN PHYSICS, 1981, 30 (02) :139-326

[9]

DRESSELHAUS MS, 1996, SCI FULLERENES CARBO, P850

[10] CARBON NANOTUBES [J].

EBBESEN, TW .

ANNUAL REVIEW OF MATERIALS SCIENCE, 1994, 24 :235-264

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