Crystal structure and characterisation of cadmium cyanamide

被引：47

作者：

Baldinozzi, G

Malinowska, B ^{[1
]}

Rakib, M

Durand, G

机构：

[1] Ecole Cent Paris, Lab Chim & Genie Procedes, F-92295 Chatenay Malabry, France

[2] Ecole Cent Paris, Lab Struct Proprietes & Modelisat Solide, F-92295 Chatenay Malabry, France

来源：

JOURNAL OF MATERIALS CHEMISTRY | 2002年 / 12卷 / 02期

关键词：

D O I：

10.1039/b106498c

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

The crystal structure of cadmium cyanamide was investigated by X-ray powder analysis and refined using the Rietveld method. Very fine powders of CdCN2 in the nanometre range were obtained by chemical bath deposition. The size, shape and microstrain were characterised by X-ray diffraction and transmission electron microscopy. The refined structure is very close to that of MgCN2. Infrared spectroscopy and thermogravimetric analysis were also performed to fully characterise the compound.

引用

页码：268 / 272

页数：5

共 26 条

[1] ORIGINAL HIGHLY ACCURATE GONIOMETER FOR X-RAY-POWDER DIFFRACTION AT CONTROLLED TEMPERATURE [J].