Powder structure determination of Li2PdO3:: a NaCl structure type with turbostratic effect

被引:5
作者
Laligant, Y
Lacorre, P
Rodríquez-Carvajal, J
机构
[1] Univ Maine, Lab Fluorures, CNRS, ESA, FR-72085 Le Mans 9, France
[2] CEA Saclay, CNRS, Lab Leon Brillouin, FR-91191 Gif Sur Yvette, France
来源
EPDIC 7: EUROPEAN POWDER DIFFRACTION, PTS 1 AND 2 | 2001年 / 378-3卷
关键词
powder diffraction; structure solution; turbostratic effect; warren profile;
D O I
10.4028/www.scientific.net/MSF.378-381.632
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The compound Li2PdO3 has been synthesised uder oxygen pressure. The crystal structure of this palladate was investigated using X-ray powder diffraction and electron microscopy. Li2PdO3 crystallises with the Li5ReO6-type structure in the C2/m space group with a = 5.1207(6), b = 8.844(1), c = 5.1095(3)Angstrom and beta = 109.559(8)degrees. 2D Disorder in Li2PdO3 induces Warren effect on the diffraction peaks in the c direction.
引用
收藏
页码:632 / 637
页数:6
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