Synthesis of magnetite nanoparticles in W/O microemulsion

被引:118
作者
Liu, ZL [1 ]
Wang, X
Yao, KL
Du, GH
Lu, QH
Ding, ZH
Tao, J
Ning, Q
Luo, XP
Tian, DY
Xi, D
机构
[1] Huazhong Univ Sci & Technol, Dept Phys, Wuhan 430074, Peoples R China
[2] Huazhong Univ Sci & Technol, State Key Lab Laser Technol, Wuhan 430074, Peoples R China
[3] Chinese Acad Sci, Int Ctr Mat Phys, Shenyang 110015, Peoples R China
[4] Tongji Med Coll, Wuhan 430030, Peoples R China
关键词
D O I
10.1023/B:JMSC.0000020046.68106.22
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The synthesis of magnetite nanoparticles in W/O microemulsion is discussed. In this method, a single microemulsion is used as reaction mediator. The structure and composition of particles are characterized by X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR), which shows the sample is composed of magnetite. From the transmission electron microscopy (TEM) image , it is found that the particle size distributions are consistently narrow and the shape of the particle is approximately spherical.
引用
收藏
页码:2633 / 2636
页数:4
相关论文
共 16 条
[1]   MAGNETIC-PROPERTIES OF MAGNETITE ULTRAFINE PARTICLES PREPARED BY W/O MICROEMULSION METHOD [J].
BANDOW, S ;
KIMURA, K ;
KONNO, K ;
KITAHARA, A .
JAPANESE JOURNAL OF APPLIED PHYSICS PART 1-REGULAR PAPERS SHORT NOTES & REVIEW PAPERS, 1987, 26 (05) :713-717
[2]  
CATTENOM TG, 1993, MATER LETT, V18, P151
[3]   Preparation of acicular gamma-Fe2O3 particles from a microemulsion-mediated reaction [J].
Chhabra, V ;
Ayyub, P ;
Chattopadhyay, S ;
Maitra, AN .
MATERIALS LETTERS, 1996, 26 (1-2) :21-26
[4]   A new simple hydrothermal preparation of nanocrystalline magnetite Fe3O4 [J].
Fan, R ;
Chen, XH ;
Gui, Z ;
Liu, L ;
Chen, ZY .
MATERIALS RESEARCH BULLETIN, 2001, 36 (3-4) :497-502
[5]   The reactivity of a Fe-Ti-O mixed oxide under different atmospheres: study of the interaction with simple alcohol molecules [J].
Glisenti, A .
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2000, 153 (1-2) :169-190
[6]  
HATRIDGE A, 1997, J MAGN MAGN MATER, V176, pL89
[7]   Microwave hydrothermal preparation of submicron-sized spherical magnetite (Fe3O4)powders [J].
Khollam, YB ;
Dhage, SR ;
Potdar, HS ;
Deshpande, SB ;
Bakare, PP ;
Kulkarni, SD ;
Date, SK .
MATERIALS LETTERS, 2002, 56 (04) :571-577
[8]   Preparation of thermo-sensitive magnetic microspheres and their application to bioprocesses [J].
Kondo, A ;
Fukuda, H .
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 1999, 153 (1-3) :435-438
[9]   Corrosion product analysis of corrosion resistant ancient Indian iron [J].
Kumar, AVR ;
Balasubramaniam, R .
CORROSION SCIENCE, 1998, 40 (07) :1169-1178
[10]   A comparison of coprecipitation with microemulsion methods in the preparation of magnetite [J].
Lee, HS ;
Lee, WC ;
Furubayashi, T .
JOURNAL OF APPLIED PHYSICS, 1999, 85 (08) :5231-5233