Synthesis of MoSe2 nanocrystallites by a solvothermal conversion from MoO3

被引：39

作者：

Zhan, JH

Zhang, ZD

Qian, XF

Wang, C

Xie, Y

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 1999年 / 34卷 / 04期

关键词：

chalcogenides; nanostructures; layered compounds; chemical synthesis;

D O I：

10.1016/S0025-5408(99)00048-3

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Nanocrystalline 2H-MoSe2 was prepared from MoO3, N2H4. H2O, and Se in pyridine at 300 degrees C for 12 h by a solvothermal method. A gray-black product was collected and characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM) analysis. The XRD pattern showed that a phase-pure product was prepared. TEM analysis showed that the product was polycrystalline and had plate-shaped particles with a diameter of about 40 nm. The conversion process from MoO3 to MoSe2 is discussed. (C) 1999 Elsevier Science Ltd.

引用

页码：497 / 501

页数：5

共 15 条

[1] RAPID SOLID-STATE SYNTHESIS OF MATERIALS FROM MOLYBDENUM-DISULFIDE TO REFRACTORIES [J].