H-2->H-1 cross-polarization in deuterated glycine

被引：4

作者：

Kolodziejski, W

Corma, A

机构：

[1] Inst. de Tecn. Quim. UPV-CSIC, Univ. Politécnica de Valencia, 46022 Valencia, Avenida de los Naranjos, s/n.

来源：

SOLID STATE NUCLEAR MAGNETIC RESONANCE | 1996年 / 7卷 / 01期

关键词：

solid state nuclear magnetic resonance; H-1 nuclear magnetic resonance; H-2->H-1 cross-polarization; spin dynamics; glycine;

D O I：

10.1016/0926-2040(96)01240-4

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

H-1 spectral details and CP kinetics are discussed. We recommend perdeuterated polycrystalline glycine as a standard for setting H-2 --> H-1 cross-polarization (CP), for H-1 chemical shift referencing and for checking the setting of the magic angle and the shims.

引用

页码：67 / 72

页数：6

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