Synthesis and characterization of ZnS nanoparticles in water/AOT/n-heptane microemulsions

被引：84

作者：

Liveri, VT

Rossi, M

D'Arrigo, G

Manno, D

Micocci, G

机构：

[1] Univ Palermo, Dipartimento Chim Fis, I-90123 Palermo, Italy

[2] Univ Rome, Dipartimento Energet, I-00161 Rome, Italy

[3] INFM, UdR Romal, I-00161 Rome, Italy

[4] Univ Lecce, Dipartimento Sci Mat, I-73100 Lecce, Italy

[5] INFM, UdR Lecce, I-73100 Lecce, Italy

来源：

APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 1999年 / 69卷 / 04期

关键词：

D O I：

10.1007/s003390051016

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

ZnS nanoparticles were synthetized using water-containing AOT reversed micelles as nanoreactors and characterized by UV-Vis spectrophotometry, HRTEM (high-resolution transmission electron microscopy), SAED (selected-area electron diffraction), and digital image processing. The experimental data evidence a slow growing process of fractal-like ZnS nanoparticles' coupled with a change of their photophysical properties. Both these processes are well described by power laws. The nanoparticles size is mainly controlled by the micellar size. After evaporation of the organic solvent, it has been found that the deposit is constituted by smaller and more stable ZnS nanoparticles bathed in a surfactant matrix.

引用

页码：369 / 373

页数：5

共 10 条

[1] Calorimetric investigation of the formation of ZnS nanoparticles in W/O microemulsions [J].