Cross-section structure of cylindrical and polymer-like micelles from small-angle scattering data .1. Test of analysis methods

被引:62
作者
Pedersen, JS [1 ]
Schurtenberger, P [1 ]
机构
[1] ETH ZURICH,INST POLYMERE,CH-8092 ZURICH,SWITZERLAND
关键词
D O I
10.1107/S0021889896006589
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The application of the indirect Fourier transformation method and the square-root deconvolution procedure of Glatter [Glatter (1977). J. Appl. Cryst. 10, 415-421; Glatter (1981). J. Appl. Cryst. 14, 101-108] for a determination of the cross-section structure of cylindrical and polymer-like micelles is investigated. The data analysis methods assume: (i) the rod-like structures are infinitely long and straight; (ii) the particles have cylindrical symmetry; (iii) the particles are monodisperse in the cross-section size and have no fluctuations in the cross-section structure. The influence of the violations of these assumptions on the applicability of the methods and the limitations have been investigated by analyzing series of simulated scattering data. In addition, the influence of finite range of scattering vectors for the data and the presence of diffuse correlations along the rod-like particles have been determined.
引用
收藏
页码:646 / 661
页数:16
相关论文
共 33 条
[1]  
Benoit H., 1953, J PHYS CHEM, V57, P958
[2]   MOLECULAR-WEIGHT DETERMINATION BY LIGHT SCATTERING [J].
DEBYE, P .
JOURNAL OF PHYSICAL AND COLLOID CHEMISTRY, 1947, 51 (01) :18-32
[3]   SHAPE AND SIZE FLUCTUATIONS OF MICROEMULSION DROPLETS - THE ROLE OF COSURFACTANT [J].
FARAGO, B ;
RICHTER, D ;
HUANG, JS ;
SAFRAN, SA ;
MILNER, ST .
PHYSICAL REVIEW LETTERS, 1990, 65 (26) :3348-3351
[5]   NEW METHOD FOR EVALUATION OF SMALL-ANGLE SCATTERING DATA [J].
GLATTER, O .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1977, 10 (OCT1) :415-421
[6]   CONVOLUTION SQUARE ROOT OF BAND-LIMITED SYMMETRICAL FUNCTIONS AND ITS APPLICATION TO SMALL-ANGLE SCATTERING DATA [J].
GLATTER, O .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1981, 14 (APR) :101-108
[7]   EVALUATION OF SMALL-ANGLE SCATTERING DATA FROM LAMELLAR AND CYLINDRICAL PARTICLES BY THE INDIRECT TRANSFORMATION METHOD [J].
GLATTER, O .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1980, 13 (DEC) :577-584
[8]   IMPROVEMENTS IN REAL-SPACE DECONVOLUTION OF SMALL-ANGLE SCATTERING DATA [J].
GLATTER, O ;
HAINISCH, B .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1984, 17 (DEC) :435-441
[9]   THE STRUCTURE OF INTERMEDIATE RIBBON PHASES IN SURFACTANT SYSTEMS [J].
HAGSLATT, H ;
SODERMAN, O ;
JONSSON, B .
LIQUID CRYSTALS, 1992, 12 (04) :667-688
[10]  
HAGSLATT H, 1994, THESIS LUND U SWEDEN