Complete resolution of Si-O-Si and Si-O-Al fragments in an aluminosilicate glass by O-17 multiple quantum magic angle spinning NMR spectroscopy

被引:153
作者
Dirken, PJ
Kohn, SC
Smith, ME
vanEck, ERH
机构
[1] UNIV KENT,DEPT PHYS,CANTERBURY CT2 7NR,KENT,ENGLAND
[2] UNIV BRISTOL,DEPT GEOL,BRISTOL BS8 1RJ,AVON,ENGLAND
关键词
D O I
10.1016/S0009-2614(97)00041-9
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Complete NMR resolution of Si-O-Si and Si-O-Al species in an aluminosilicate glass (NaAlSi3O8) is shown using O-17 multiple quantum magic angle spinning (MAS) NMR and indicates that no Al-O-Al is present at the detection limit of 0.5%.
引用
收藏
页码:568 / 574
页数:7
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