Crystal structures of methanol and ethanol solvates of secalonic acid D

被引：3

作者：

Barnes, CL ^{[1
]}

Ubillas, R

Tempesta, MS

机构：

[1] Univ Missouri, Dept Chem, Columbia, MO 65211 USA

[2] Phytera, Worcester, MA 01605 USA

[3] Nat Prod Consulting Serv, El Granada, CA 94018 USA

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 1999年 / 29卷 / 09期

关键词：

crystal structures; secalonic acid; fungi;

D O I：

10.1023/A:1009576817952

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The methanol and ethanol solvates of secalonic acid D (SAD) share the same packing pattern exhibited by the acetic acid solvate of secalonic acid A, the enantiomer of SAD. Both solvates crystallize in space group C2, with a = 17.648(2), b = 7.0897(10), c = 13.060(2) Angstrom and beta = 93.482(2)degrees for the methanol form, and a = 18.010(4), b = 7.395(2), c = 13.053(3) Angstrom and beta = 96.882(4)degrees for the ethanol form.

引用

页码：1031 / 1035

页数：5

共 12 条

[1] SECALONIC ACIDS D AND F ARE TOXIC METABOLITES OF ASPERGILLUS-ACULEATUS [J].

ANDERSEN, R ;

BUCHI, G ;

KOBBE, B ;

DEMAIN, AL .

JOURNAL OF ORGANIC CHEMISTRY, 1977, 42 (02) :352-353

[2]

BARBOUR LJ, 1999, UNPUB X SEED

[3]

Burnett M.N., 1996, ORTEP-III: Oak Ridge Thermal Ellipsoid Plot Program for Crystal Structure Illustrations

[4]

Farrugia L.J., 1997, J APPL CRYSTALLOGR, V30, P565

[5] MUTTERKORN-FARBSTOFFE .12. TRENNUNG STRUKTUR UND ABSOLUTE KONFIGURATION DER DIASTEREOMEREN SECALONSAUREN A B UND C [J].

FRANCK, B ;

GOTTSCHALK, EM ;

OHNSORGE, U ;

HUPER, F .

CHEMISCHE BERICHTE-RECUEIL, 1966, 99 (12) :3842-+

[6]

Fujimoto Y., 1983, P JPN ASS MYCOTOXICO, V17, P52

[7] ISOLATION OF A NEW SECALONIC ACID [J].

HOWARD, CC ;

JOHNSTONE, RA .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1973, (14) :464-464

[8] FUNGAL METABOLITES .6. CRYSTAL AND MOLECULAR-STRUCTURE OF SECALONIC ACID A [J].

HOWARD, CC ;

JOHNSTONE, RAW ;

KING, TJ ;

LESSINGER, L .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1976, (17) :1820-1822

[9]

KUROBANE I, 1978, TETRAHEDRON LETT, V47, P4633

[10] TERATOGENICITY OF SECALONIC ACID-D IN MICE [J].

REDDY, CS ;

REDDY, RV ;

HAYES, AW ;

CIEGLER, A .

JOURNAL OF TOXICOLOGY AND ENVIRONMENTAL HEALTH, 1981, 7 (3-4) :445-455

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