The preparation of yttrium oxide film deposited by electrochemical method

被引:29
作者
Lee, J [1 ]
Tak, Y [1 ]
机构
[1] Inha Univ, Dept Chem Engn, Inchon 402751, South Korea
关键词
yttrium oxide; yttrium hydroxide; electrochemical preparation; EQCM; dehydration;
D O I
10.1258/1357633991933233
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Yttrium oxide films were prepared on indium-tin-oxide (ITO) by electrochemical method followed by heat treatment. During electrochemical reduction, a thin film of yttrium hydroxide was initially formed and vertically oriented growth bands were developed. Structural and morphological changes occurring during the deposition and dehydration of yttrium hydroxides were investigated by use of XRD, SEM and TG/DTA. The extent of dehydration increased with temperature. Y(OH)(3) phase transformed to alpha-Y(OH)(3) at about 400 degrees C, and then Y2O3 above 450 degrees C.
引用
收藏
页码:139 / 142
页数:4
相关论文
共 17 条
[1]  
ATKINS PW, 1989, GEN CHEM, P927
[2]   ELECTROCHEMICAL APPLICATIONS OF THE QUARTZ CRYSTAL MICROBALANCE [J].
DEAKIN, MR ;
BUTTRY, DA .
ANALYTICAL CHEMISTRY, 1989, 61 (20) :A1147-+
[3]   ELECTROLYTIC ZRO2 COATINGS .1. ELECTROCHEMICAL ASPECTS [J].
GALOR, L ;
SILBERMAN, I ;
CHAIM, R .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1991, 138 (07) :1939-1942
[4]   Electrochemical deposition of copper(I) oxide films [J].
Golden, TD ;
Shumsky, MG ;
Zhou, YC ;
VanderWerf, RA ;
VanLeeuwen, RA ;
Switzer, JA .
CHEMISTRY OF MATERIALS, 1996, 8 (10) :2499-2504
[5]  
GURVITCH M, 1987, APPL PHYS LETT, V51
[6]   Electrolyte optimization for cathodic growth of zinc oxide films [J].
Izaki, M ;
Omi, T .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1996, 143 (03) :L53-L55
[7]  
Lee J, 1998, MATER RES SOC SYMP P, V495, P457
[8]   Improvement in electrochromic stability of electrodeposited nickel hydroxide thin film [J].
Natarajan, C ;
Matsumoto, H ;
Nogami, G .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1997, 144 (01) :121-126
[9]  
Nyquist R.A., 1997, HDB INFRARED RAMAN S, V4, P223
[10]   DIELECTRIC-PROPERTIES OF RF-SPUTTERED Y2O3 THIN-FILMS [J].
ONISAWA, K ;
FUYAMA, M ;
TAMURA, K ;
TAGUCHI, K ;
NAKAYAMA, T ;
ONO, YA .
JOURNAL OF APPLIED PHYSICS, 1990, 68 (02) :719-723