Desorption electrospray ionization and electrosonic spray ionization for solid- and solution-phase analysis of industrial polymers

被引:63
作者
Nefliu, M [1 ]
Venter, A [1 ]
Cooks, RG [1 ]
机构
[1] Purdue Univ, Dept Chem, W Lafayette, IN 47907 USA
关键词
D O I
10.1039/b514057a
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Desorption electrospray ionization (DESI) and electrosonic spray ionization (ESSI), two new techniques, are used to measure average molecular weights and molecular weight distributions of solid-phase and solution-phase samples of the same polymers.
引用
收藏
页码:888 / 890
页数:3
相关论文
共 24 条
[1]   MASS-SPECTROMETRY OF SYNTHETIC-POLYMERS BY UV MATRIX-ASSISTED LASER DESORPTION IONIZATION [J].
BAHR, U ;
DEPPE, A ;
KARAS, M ;
HILLENKAMP, F ;
GIESSMANN, U .
ANALYTICAL CHEMISTRY, 1992, 64 (22) :2866-2869
[2]   Analysis of polyethylene by using cyclopentadienyl cobalt chemical ionization combined with laser-induced acoustic desorption/Fourier transform ion cyclotron resonance mass spectrometry [J].
Campbell, JL ;
Fiddler, MN ;
Crawford, KE ;
Gqamana, PP ;
Kenttämaa, HI .
ANALYTICAL CHEMISTRY, 2005, 77 (13) :4020-4026
[3]   Quantitative analysis of polyethylene blends by Fourier transform infrared spectroscopy [J].
Cran, MJ ;
Bigger, SW .
APPLIED SPECTROSCOPY, 2003, 57 (08) :928-932
[4]   ELECTROSPRAY IONIZATION-PRINCIPLES AND PRACTICE [J].
FENN, JB ;
MANN, M ;
MENG, CK ;
WONG, SF ;
WHITEHOUSE, CM .
MASS SPECTROMETRY REVIEWS, 1990, 9 (01) :37-70
[5]  
Guittard J, 1996, J MASS SPECTROM, V31, P1409, DOI 10.1002/(SICI)1096-9888(199612)31:12<1409::AID-JMS440>3.3.CO
[6]  
2-K
[7]   Probing the effects of cone potential in the electrospray ion source: Consequences for the determination of molecular weight distributions of synthetic polymers [J].
Hunt, SM ;
Sheil, MM ;
Belov, M ;
Derrick, PJ .
ANALYTICAL CHEMISTRY, 1998, 70 (09) :1812-1822
[8]  
IOANNIS VB, 1987, MACROMOLECULES, V20, P407
[9]  
Jackson AT, 1998, RAPID COMMUN MASS SP, V12, P1914, DOI 10.1002/(SICI)1097-0231(19981215)12:23<1914::AID-RCM400>3.0.CO
[10]  
2-N