Nanocrystalline zirconia surface-doped with alumina:: Chemical vapor synthesis, characterization, and properties

被引:33
作者
Srdic, VV [1 ]
Winterer, M
Möller, A
Miehe, G
Hahn, H
机构
[1] Tech Univ Darmstadt, Dept Mat Sci, Div Thin Film, Darmstadt, Germany
[2] Tech Univ Darmstadt, Dept Mat Sci, Struct Res Div, Darmstadt, Germany
关键词
D O I
10.1111/j.1151-2916.2001.tb01093.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Nanocrystalline zirconia with a grain size of similar to5 run was surface-doped with 3 and 30 mol% alumina by chemical vapor synthesis using two sequential hot-wall reactors. The powders were characterized by high-resolution transmission electron microscopy, X-ray diffractometry (XRD), and nitrogen adsorption. Aqueous dispersions were studied by zeta-potential measurements and photocorrelation spectroscopy. Green and sintered ceramic bodies were investigated by high-resolution scanning electron microscopy, XRD, and nitrogen adsorption. Zirconia surface-doped with 3 mol% of alumina displays substantial changes in dispersability and sinterability compared with pure nanocrystalline zirconia.
引用
收藏
页码:2771 / 2776
页数:6
相关论文
共 20 条
[1]   THE DETERMINATION OF PORE VOLUME AND AREA DISTRIBUTIONS IN POROUS SUBSTANCES .1. COMPUTATIONS FROM NITROGEN ISOTHERMS [J].
BARRETT, EP ;
JOYNER, LG ;
HALENDA, PP .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1951, 73 (01) :373-380
[2]  
BRINKER CJ, 1990, SOL GEL SCI, P519
[3]  
Chu B., 1991, LASER LIGHT SCATTERI, V2nd
[4]  
CULLITY AD, 1978, ELEMENTS XRAY DIFFRA
[5]  
David Kingery W., 1976, INTRO CERAMICS, V17
[6]   Sequential gas-phase formation of Al2O3 and SiO2 layers on aerosol-made TiO2 particles [J].
Fotou, GP ;
Kodas, TT .
ADVANCED MATERIALS, 1997, 9 (05) :420-&
[7]   STABILIZATION OF TETRAGONAL STRUCTURE IN ZIRCONIA MICROCRYSTALS [J].
GARVIE, RC .
JOURNAL OF PHYSICAL CHEMISTRY, 1978, 82 (02) :218-224
[8]   STRUCTURES OF THE ZRO2 POLYMORPHS AT ROOM-TEMPERATURE BY HIGH-RESOLUTION NEUTRON POWDER DIFFRACTION [J].
HOWARD, CJ ;
HILL, RJ ;
REICHERT, BE .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1988, 44 :116-120
[9]  
KINGERY WD, 1967, SINTERING RELATED PH, P23
[10]   FORMATION OF NEW ACID SITES IN DILUTE OXIDE SOLID-SOLUTIONS - A PREDICTIVE MODEL [J].
KUNG, HH .
JOURNAL OF SOLID STATE CHEMISTRY, 1984, 52 (02) :191-196