Poly(2,5-di-(-2-thienyl)-pyrrole) films anodically synthesized on Pt from 5 mM monomer + 0.1 M LiClO4 + CH3CN at 0.5 mA cm(-2) were reduced in water + CH3CN (3:2) with 0.1 M LiClO4 at -200 mVvs. SSCE. The capacitance and charge storage capacity of cm these reduced films and some oxidized films in the same medium were determined by electrochemical impedance spectroscopy (EIS).