Conversion of the oldest XAFS station at the first dedicated SR source to a state-of-the-art XAFS facility

被引:6
作者
Cheung, KC [1 ]
Strange, R
Harvey, I
Dobson, B
Derbyshire, G
Kay, J
Binsted, N
Linford, R
Hasnain, S
机构
[1] De Montfort Univ, Fac Sci Appl, Leicester LE1 9BH, Leics, England
[2] Daresbury Lab, CCLRC, Warrington WA4 4AD, Cheshire, England
[3] Rutherford Appleton Lab, CCLRC, Didcot OX11 0QX, Oxon, England
关键词
XAFS; EXAFS; QuEXAFS; monochromator; optics; stopped-flow; instrumentation;
D O I
10.1107/S0909049598016860
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Station 7.1 was the first XAFS station to operate at the Synchrotron Radiation Source (SRS) starting in 1981. A major upgrade of 7.1 has been taking place aimed towards a multidimensional XAFS and single crystal facility for 3d elements (Ca to Zn). The optical upgrade included a collimating mirror and QuEXAFS monochromator, also a highly compact and rapid count-rate multi-element solid state detector has been designed, built and recently commissioned. A stopped-flow system is commissioned and a diffractometer stage is planned. The necessary analytical tools for 3D XAFS refinement using crystallographic data as the starting 3D model have been developed for solution XAFS.
引用
收藏
页码:161 / 163
页数:3
相关论文
共 10 条
  • [1] State-of-the-art analysis of whole X-ray absorption spectra
    Binsted, N
    Hasnain, SS
    [J]. JOURNAL OF SYNCHROTRON RADIATION, 1996, 3 : 185 - 196
  • [2] AN EXTENDED-X-RAY-ABSORPTION-FINE-STRUCTURE STUDY OF BOVINE ERYTHROCYTE SUPEROXIDE-DISMUTASE IN AQUEOUS-SOLUTION - DIRECT EVIDENCE FOR 3-CO-ORDINATE CU(I) IN REDUCED ENZYME
    BLACKBURN, NJ
    HASNAIN, SS
    BINSTED, N
    DIAKUN, GP
    GARNER, CD
    KNOWLES, PF
    [J]. BIOCHEMICAL JOURNAL, 1984, 219 (03) : 985 - 990
  • [3] CHEUNG KC, 1998, THESIS DE MONTFORD U
  • [4] NEAR-EDGE X-RAY ABSORPTION-SPECTRA FOR METALLIC CU AND MN
    GREAVES, GN
    DURHAM, PJ
    DIAKUN, G
    QUINN, P
    [J]. NATURE, 1981, 294 (5837) : 139 - 142
  • [5] FLUORESCENCE EXAFS AT THE SRS - INCREASED SENSITIVITY FOR DILUTE SAMPLES
    HASNAIN, SS
    QUINN, PD
    DIAKUN, GP
    WARDELL, EM
    GARNER, CD
    [J]. JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS, 1984, 17 (01): : 40 - 43
  • [6] IN-LABORATORY STOPPED-FLOW EXTENDED X-RAY-ABSORPTION FINE-STRUCTURE APPARATUS IN THE DISPERSIVE MODE FOR DETERMINATION OF THE STRUCTURE OF SHORT-LIVED INTERMEDIATES
    INADA, Y
    FUNAHASHI, S
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1994, 65 (01) : 18 - 24
  • [7] Synchrotron radiation research in the UK
    Munro, IH
    [J]. JOURNAL OF SYNCHROTRON RADIATION, 1997, 4 : 344 - 358
  • [8] QUICK FLUORESCENCE EXAFS - AN IMPROVED METHOD FOR COLLECTION OF CONVENTIONAL XAFS DATA AND FOR STUDYING REACTION INTERMEDIATES IN DILUTE SYSTEMS
    MURPHY, LM
    DOBSON, BR
    NEU, M
    RAMSDALE, CA
    STRANGE, RW
    HASNAIN, SS
    [J]. JOURNAL OF SYNCHROTRON RADIATION, 1995, 2 : 64 - 69
  • [9] A critical assessment of the evidence from XAFS and crystallography for the breakage of the imidazolate bridge during catalysis in CuZn superoxide dismutase
    Murphy, LM
    Strange, RW
    Hasnain, SS
    [J]. STRUCTURE, 1997, 5 (03) : 371 - 379
  • [10] A SLITLESS DOUBLE CRYSTAL MONOCHROMATOR FOR EXAFS AND XANES MEASUREMENTS
    VANDERHOEK, MJ
    WERNER, W
    VANZUYLEN, P
    DOBSON, BR
    HASNAIN, SS
    WORGAN, JS
    LUIJCKX, G
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1986, 246 (1-3) : 380 - 384