Thermal stability of nanocrystalline Sm2O3 and Sm2O3-MgO

被引:14
作者
Sieger, H
Suffner, J
Hahn, H
Raju, AR
Miehe, G
机构
[1] Tech Univ Darmstadt, Joint Res Lab Nanomat, D-64287 Darmstadt, Germany
[2] Forschungszentrum Karlsruhe, D-64287 Darmstadt, Germany
[3] Jawaharlal Nehru Ctr Adv Sci Res, Bangalore 560064, Karnataka, India
[4] Tech Univ Darmstadt, Struct Res Div, Inst Sci Mat, D-64287 Darmstadt, Germany
关键词
D O I
10.1111/j.1551-2916.2005.00840.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Nanocrystalline Sm2O3 and Sm2O3-MgO powders have been prepared by spray pyrolysis of aqueous precursor solutions containing citric acid as a complexant. Synthesized powders consist of hollow spheres with thin shells. The two-phase samples exhibit an improved microstructural stability compared with pure Sm2O3. The microstructure before and after various heat treatments has been investigated by high-resolution transmission electron microscopy, scanning electron microscopy, nitrogen adsorption, and X-ray diffraction.
引用
收藏
页码:979 / 984
页数:6
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