Accelerated solvent extraction of herbicides in agricultural soil samples

被引：9

作者：

Guzzella, L ^{[1
]}

Pozzoni, F ^{[1
]}

机构：

[1] CNR, Ist Ricerca Sulle Acque, I-20047 Brugherio, Milan, Italy

来源：

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY | 1999年 / 74卷 / 1-4期

关键词：

herbicides; soil; extraction; Soxhlet; accelerated solvent extraction;

D O I：

10.1080/03067319908031420

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This study was undertaken for comparing the standard Soxhlet procedure with an Accelerated Solvent Extraction (ASE), an extraction procedure already accepted by the US EPA that uses organic solvents at high temperatures and pressures. Soil samples contaminated by atrazine, terbuthylazine, alachlor and metolachlor herbicides and by their main transformation products were utilised for this comparison. The soil samples were selected on the basis of different textural characteristics and organic carbon contents. The obtained results showed good recovery efficiency of the ASE technique, reducing extraction times and organic solvent usage.

引用

页码：123 / 133

页数：11

共 13 条

[1]

*DION, 1995, 322 DION

[2]

*DION, 1995, 313 DION

[3]

*DION, 1995, 319 DION

[4]

*DION, 1995, 320 DION

[5]

*DION, 1995, 317 DION

[6]

*DION, 1995, 318 DION

[7]

GANDER K, 1986, J CHROMATOGR, V371, P299

[8] Migration of pesticide residues from agricultural soil to groundwater [J].

Guzzella, L ;

DePaolis, A ;

Bartone, C ;

Pozzoni, F ;

Giuliano, G .

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1996, 65 (1-4) :261-275

[9] ANALYTICAL-SCALE SUPERCRITICAL FLUID EXTRACTION [J].

HAWTHORNE, SB .

ANALYTICAL CHEMISTRY, 1990, 62 (11) :A633-&

[10] MICROWAVE-ENERGY FOR ACID DECOMPOSITION AT ELEVATED-TEMPERATURES AND PRESSURES USING BIOLOGICAL AND BOTANICAL SAMPLES [J].

KINGSTON, HM ;

JASSIE, LB .

ANALYTICAL CHEMISTRY, 1986, 58 (12) :2534-2541

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