Enhanced resolution in MAS NMR for combinatorial chemistry

被引：49

作者：

Shapiro, MJ

Chin, J

Marti, RE

Jarosinski, MA

机构：

[1] SANDOZ INC,RES INST,SANDOZ PHARMACEUT CORP,ONCOL RES PROGRAM,E HANOVER,NJ 07936

[2] SANDOZ INC,RES INST,SANDOZ PHARMACEUT CORP,PRECLIN RES,E HANOVER,NJ 07936

来源：

TETRAHEDRON LETTERS | 1997年 / 38卷 / 08期

关键词：

D O I：

10.1016/S0040-4039(97)00092-0

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

We have demonstrated the ability to obtain high resolution NMR spectra from samples on resin using J-resolved 2D NMR. Projection of the non-tilted spectrum onto the chemical shift dimension provides enhanced resolution and virtually complete disappearance of the polymer resonances. (C) 1997 Elsevier Science Ltd.

引用

页码：1333 / 1336

页数：4

共 9 条

[1] STRUCTURE DETERMINATION IN COMBINATORIAL CHEMISTRY - UTILIZATION OF MAGIC-ANGLE-SPINNING HMQC AND TOCSY NMR-SPECTRA IN THE STRUCTURE DETERMINATION OF WANG-BOUND LYSINE [J].