Characterization of coating systems by scanning acoustic microscopy: Debonding, blistering and surface topology

被引:32
作者
Alig, Ingo [1 ]
Tadjbach, Sascha [2 ]
Krueger, Peter [2 ]
Oehler, Harald [1 ]
Lellinger, Dirk [1 ]
机构
[1] Deutsch Kunststoff Inst Darmstadt, D-64289 Darmstadt, Germany
[2] Bayer MaterialSci, D-51368 Leverkusen, Germany
关键词
Scanning acoustic microscopy; Coatings; Adhesives; Defects; Weathering and corrosion tests; THIN POLYMER-FILMS; ORGANIC COATINGS; LIQUID-FILMS; PHASE-SEPARATION; KELVIN PROBE; INSTABILITY; DEGRADATION; MORPHOLOGY; KINETICS; DEFECTS;
D O I
10.1016/j.porgcoat.2008.09.013
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Scanning acoustic microscopy (SAM) has been applied to different commercial coating systems on steel substrates in order to evaluate the potential of the method for fast non-destructive testing during material development: the focus was on defect detection after and during accelerated weathering and corrosion tests. The possibility of detecting hidden defects (e.g., blisters) in an early stage of weathering or corrosion tests has been evaluated for different commercial coating systems. Using different scanning modes 2K polyurethane systems (solvent- and water-borne) have been examined by SAM. Debonding at the polymer/substrate interface and the interface between base coat and top coat has been studied in samples after simulated weathering. The time dependence of "blister nucleation and growth" has been studied during a salt spray test. Furthermore, the surface topography has been investigated for UV-cured acrylic systems with and without antioxidants after simulated weathering. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:112 / 119
页数:8
相关论文
共 33 条
[1]  
ADDISON RC, 1988, P IEEE ULTR S, P739
[2]   Monitoring of film formation, curing and ageing of coatings by an ultrasonic reflection method [J].
Alig, I. ;
Oehler, H. ;
Lellinger, D. ;
Tadjbach, S. .
PROGRESS IN ORGANIC COATINGS, 2007, 58 (2-3) :200-208
[3]   Kinetics and morphology of phase separation in fluids: The role of droplet coalescence [J].
Beysens, DA .
PHYSICA A, 1997, 239 (1-3) :329-339
[4]  
BINDER K, 1990, MATERIAALS SCI TECHN, V5, pCH7
[5]   Dewetting modes of thin metallic films: Nucleation of holes and spinodal dewetting [J].
Bischof, J ;
Scherer, D ;
Herminghaus, S ;
Leiderer, P .
PHYSICAL REVIEW LETTERS, 1996, 77 (08) :1536-1539
[6]   Study of the coating/substrate interface by scanning acoustic microscopy - Cathodic disbonding of epoxy-polyamide lacquer from mild steel [J].
Crossen, JD ;
Sykes, JM ;
Zhai, T ;
Briggs, GAD .
FARADAY DISCUSSIONS, 1997, 107 :417-424
[7]  
Ferry J. D., 1961, VISCOELASTIC PROPERT
[8]  
Gunton J., 1983, PHASE TRANSITIONS CR, V8
[9]  
HASHIMOTO T, 1993, MAT SCI TECHNOLOGY, V12, pCH6
[10]   Spinodal dewetting in liquid crystal and liquid metal films [J].
Herminghaus, S ;
Jacobs, K ;
Mecke, K ;
Bischof, J ;
Fery, A ;
Ibn-Elhaj, M ;
Schlagowski, S .
SCIENCE, 1998, 282 (5390) :916-919