Analysis of ochratoxin A in pig kidney and rye flour using liquid chromatography tandem mass spectrometry (LC/MS/MS)

被引：28

作者：

Jorgensen, K ^{[1
]}

Vahl, M ^{[1
]}

机构：

[1] Inst Food Res & Nutr, Danish Vet & Food Adm, DK-2860 Soborg, Denmark

来源：

FOOD ADDITIVES AND CONTAMINANTS | 1999年 / 16卷 / 11期

关键词：

ochratoxin A; liquid chromatography; tandem mass spectrometry; pig kidney; rye flour;

D O I：

10.1080/026520399283731

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

A liquid chromatography electrospray tandem mass spectrometric (LC/MS/MS) method is described for analysis and confirmation of ochratoxin A in pig kidney and rye flour using derivatization of ochratoxin A to the methyl ester. Ochratoxin A methyl(d(3))ester is used as internal standard. The method works well, the detection limit is 0.02 mu g/kg and the repeatability (coefficient of variation) is between 6% and 16% in the contamination range 0.5 to 8 mu g/kg.

引用

页码：451 / 456

页数：6

共 9 条

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