Sonochemical synthesis of silver, copper and lead selenides

被引:63
作者
Li, B
Xie, Y [1 ]
Huang, J
Qian, Y
机构
[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China
[3] Univ Sci & Technol China, Dept Phys Chem, Hefei 230026, Anhui, Peoples R China
基金
中国国家自然科学基金;
关键词
Ag2Se; CuSe; ethylenediamine; nanocrystalline; PbSe; sonochemistry;
D O I
10.1016/S1350-4177(99)00013-9
中图分类号
O42 [声学];
学科分类号
070206 ; 082403 ;
摘要
Ag2Se, CuSe and PbSe were prepared by irradiating the mixtures of AgNO3, CuI or PbCl2 with selenium in ethylenediamine (en) with ultrasound at 18 kHz, using a commercial ultrasonic cleaner, respectively. X-ray powder diffraction (XRD) patterns and transmission electron microscope (TEM) images show that the products are orthorhombic Ag,Se, hexagonal CuSe and cubic PbSe, respectively, and all are well crystallized in nanometers. (C) 1999 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:217 / 220
页数:4
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