Synthesis and characterization of Sb2Se3 nanorods

被引：79

作者：

Wang, JW

Deng, ZX

Li, YD ^{[1
]}

机构：

[1] Tsing Hua Univ, Key Lab Atom & Mol Nanosci, Minist Educ, Dept Chem, Beijing 100084, Peoples R China

[2] Tsing Hua Univ, Key Lab Atom & Mol Nanosci, Minist Educ, Tsinghua Foxconn Lab, Beijing 100084, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2002年 / 37卷 / 03期

基金：

中国国家自然科学基金;

关键词：

chalcogenide; nanorods; chemical synthesis;

D O I：

10.1016/S0025-5408(02)00675-X

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A hydrothermal reduction route was employed for the synthesis of Sb2Se3 Semiconductor nanorods. The reaction temperature for the formation of Sb2Se3 nanorods should be above 130degreesC, otherwise impurities, such as Sb2O3 and unreacted Se, would exist. The role of hydrazine as both the reducing agent and the coordinator was also found to be crucial for the formation of the rod-like morphologies. The products were characterized by XRD, SEM, TEM, XPS, absorption spectroscopy and Raman spectroscopy. (C) 2002 Elsevier Science Ltd. All rights reserved.

引用

页码：495 / 502

页数：8

共 23 条

[1] Semiconducting superlattices templated by molecular assemblies [J].