A versatile capillary gas chromatography inductively coupled plasma mass spectrometer interface

被引：11

作者：

Pritzl, G ^{[1
]}

StuerLauridsen, F ^{[1
]}

Carlsen, L ^{[1
]}

Jensen, AK ^{[1
]}

Thorsen, TK ^{[1
]}

机构：

[1] UNIV ROSKLIDE,INST LIFESCI & CHEM,DK-4000 ROSKILDE,DENMARK

来源：

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY | 1996年 / 62卷 / 02期

关键词：

ICP-MS; GC-ICP-MS; organometals; speciation; organotin partitioning;

D O I：

10.1080/03067319608027061

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A versatile, inexpensive, easily made interface for capillary GC-ICPMS (HRGC-ICPMS) on line coupling has been constructed. The interface does not require any changes of the ICP, and can be done in less than a minute. Optimizing of the ICP-MS and the interface can be performed on-line under GC conditions. The capability of the hyphenated system are demonstrated by analyzing standards of non-polar organometallic compounds of P, As, Sn and Sb, as well as organotins in an environmental sediment sample.

引用

页码：147 / 159

页数：13

共 26 条

[1]

[Anonymous], SEDIMENTS CHEM TOXIC

[2] NEW METHOD FOR THE PRODUCTION OF VOLATILE ORGANOMETALLIC SPECIES FOR ANALYSIS FROM THE ENVIRONMENT - SOME BUTYL TIN LEVELS IN UK SEDIMENTS [J].

ASHBY, JR ;

CRAIG, PJ .

SCIENCE OF THE TOTAL ENVIRONMENT, 1989, 78 :219-232

[3] COUPLED GAS-CHROMATOGRAPHY ATOMIC-ABSORPTION SPECTROMETRY USING SEMIENCLOSED TUBULAR ATOMIZERS - THEORETICAL-ANALYSIS OF DETECTOR PERFORMANCE-CHARACTERISTICS [J].

BAXTER, DC ;

FRECH, W .

ANALYST, 1993, 118 (05) :495-504

[4] INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY FOR ELEMENTAL ANALYSIS AND ISOTOPE RATIO DETERMINATIONS IN INDIVIDUAL ORGANIC-COMPOUNDS SEPARATED BY GAS-CHROMATOGRAPHY [J].

CHONG, NS ;

HOUK, RS .

APPLIED SPECTROSCOPY, 1987, 41 (01) :66-74

[5]

Craig, 1986, ORGANOMETALLIC COMPO

[6] ARSENIC LIPIDS IN THE DIGESTIVE GLAND OF THE WESTERN ROCK LOBSTER PANULIRUS-CYGNUS - AN INVESTIGATION BY HPLC ICP-MS [J].

EDMONDS, JS ;

SHIBATA, Y ;

FRANCESCONI, KA ;

YOSHINAGA, J ;

MORITA, M .

SCIENCE OF THE TOTAL ENVIRONMENT, 1992, 122 (03) :321-335

[7] LOW-PRESSURE INDUCTIVELY-COUPLED PLASMA SOURCE FOR MASS-SPECTROMETRY [J].

EVANS, EH ;

CARUSO, JA .

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1993, 8 (03) :427-431

[8] DETERMINATION OF VOLATILE METAL AND METALLOID COMPOUNDS IN GASES FROM DOMESTIC WASTE DEPOSITS WITH GC ICP-MS [J].

FELDMANN, J ;

GRUMPING, R ;

HIRNER, AV .

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1994, 350 (4-5) :228-234

[9] DETERMINATION OF METHYLMERCURY IN FISH SAMPLES USING GC/AA AND SODIUM TETRAETHYLBORATE DERIVATIZATION [J].

FISCHER, R ;

RAPSOMANIKIS, S ;

ANDREAE, MO .

ANALYTICAL CHEMISTRY, 1993, 65 (06) :763-766

[10] DETERMINATION OF METHYLMERCURY IN ORGANIC MATRICES WITH GAS-CHROMATOGRAPHY ATOMIC-ABSORPTION SPECTROMETRY [J].

HARMS, U .

MIKROCHIMICA ACTA, 1992, 109 (1-4) :131-132

← 1 2 3 →