Preparation of LaFeAsO0.9F0.1 wires by the powder-in-tube method

被引:61
作者
Gao, Zhaoshun [1 ]
Wang, Lei [1 ]
Qi, Yanpeng [1 ]
Wang, Dongliang [1 ]
Zhang, Xianping [1 ]
Ma, Yanwei [1 ]
机构
[1] Chinese Acad Sci, Inst Elect Engn, Key Lab Appl Superconduct, Beijing 100190, Peoples R China
关键词
D O I
10.1088/0953-2048/21/10/105024
中图分类号
O59 [应用物理学];
学科分类号
摘要
We report that Fe sheathed LaFeAsO0.9F0.1 wires with Ti as a buffer were fabricated by the powder-in-tube (PIT) method for the first time. Compared to the common two-step vacuum quartz tube synthesis method, the PIT method is more convenient and safe for synthesizing the novel iron-based layered superconductors. Structural analysis by means of x-ray diffraction shows that LaFeAsO0.9F0.1 is the main phase in wires produced by this synthesis method. The transition temperature of the LaFeAsO0.9F0.1 wire is around 25 K. The micrograph shows a homogeneous microstructure with a grain size of 1-3 mu m. The results suggest that the PIT process is promising for preparing iron-based layered superconductors.
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页数:4
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