Analytical methods for the determination of 9 antifouling paint booster biocides in estuarine water samples

被引：48

作者：

Voulvoulis, N ^{[1
]}

Scrimshaw, MD ^{[1
]}

Lester, JN ^{[1
]}

机构：

[1] Univ London Imperial Coll Sci Technol & Med, TH Huxley Sch Environm Earth Sci & Engn, Environm Proc & Water Technol Grp, London SW7 2PE, England

来源：

CHEMOSPHERE | 1999年 / 38卷 / 15期

关键词：

antifouling paint; chlorothalonil; dichlofluanid; diuron; Irgarol; 1051; Kathon; 5287; zineb; zinc; pyrithione; TCMS pyridine; TCMTB;

D O I：

10.1016/S0045-6535(98)00580-3

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

Analytical procedures for the determination of nine organic booster biocides which are currently licensed for use in marine antifouling paints, and are thought likely to occur at concentrations in the ng l(-1) range in estuarine water samples, are reviewed. A robust multiresidue method for the determination of four compounds (chlorothalonil, dichlofluanid, diuron and Irgarol 1051) is suggested. A route for the development of a method for the analysis of zinc pyrithione is outlined, based on an extraction method and subsequent derivatisation prior to determination by HPLC with fluorescence defection. Methodology for Zineb, Kathon 5287, TCMS pyridine and TCMTB is less clearly defined. (C) 1999 Elsevier Science Ltd. All rights reserved.

引用

页码：3503 / 3516

页数：14

共 73 条

[1] MULTI-RESIDUE PESTICIDE ANALYSIS IN ENVIRONMENTAL WATER SAMPLES USING SOLID-PHASE EXTRACTION DISCS AND GAS-CHROMATOGRAPHY WITH FLAME THERMIONIC AND MASS-SELECTIVE DETECTION [J].