Microimpedance - Localized material analysis

被引：32

作者：

Lohrengel, MM ^{[1
]}

Heiroth, S ^{[1
]}

Kluger, K ^{[1
]}

Pilaski, M ^{[1
]}

Walther, B ^{[1
]}

机构：

[1] Univ Dusseldorf, Inst Phys Chem, D-40225 Dusseldorf, Germany

来源：

ELECTROCHIMICA ACTA | 2006年 / 51卷 / 8-9期

关键词：

microelectrochemistry; microcell; microreactor; capillary; microimpedance;

D O I：

10.1016/j.electacta.2005.02.120

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 [应用化学];

摘要：

Many technically relevant materials are non-homogeneous in structure. Their investigation requires a locally resolved surface analysis. An exact determination of the accessed area and a potentiostatic control in a three-electrode configuration are necessary. This becomes possible by capillary-based microcells which enable local impedance measurements and even impedance mapping of the surface. Different aspects and strategies of this microimpedance spectroscopy are presented and discussed, together with some examples. (c) 2005 Elsevier Ltd. All rights reserved.

引用

页码：1431 / 1436

页数：6

共 23 条

[1]

Electrochemical characterisation of aluminium AA7075-T6 and solution heat treated AA7075 using a micro-capillary cell [J].

Andreatta, F ;

Lohrengel, MM ;

Terryn, H ;

de Wit, JHW .

ELECTROCHIMICA ACTA, 2003, 48 (20-22) :3239-3247

[2]

DAVYDOV AD, 1978, ELEKTROKHIMIYA, V14, P901

[3]

Aluminium oxide tunnel junctions: influence of preparation technique, sample geometry and oxide thickness [J].

Diesing, D ;

Hassel, AW ;

Lohrengel, MM .

THIN SOLID FILMS, 1999, 342 (1-2) :282-290

[4]

Electrochemical investigations of single microparticles [J].

Hamelmann, T ;

Lohrengel, MM .

ELECTROCHIMICA ACTA, 2001, 47 (1-2) :117-120

[5]

Localised investigation of coarse grain gold with the scanning droplet cell and by the Laue method [J].

Hassel, AW ;

Seo, M .

ELECTROCHIMICA ACTA, 1999, 44 (21-22) :3769-3777

[6]

Hassel AW, 1995, MATER SCI FORUM, V185-, P581, DOI 10.4028/www.scientific.net/MSF.185-188.581

[7]

ELECTROCHEMICAL CHARACTERIZATION OF OXIDE LAYERS ON SINGLE GRAINS OF A POLYCRYSTALLINE TI-SAMPLE [J].

KUDELKA, S ;

MICHAELIS, A ;

SCHULTZE, JW .

BERICHTE DER BUNSEN-GESELLSCHAFT-PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 1995, 99 (08) :1020-1027

[8]

THE NORMAL MEMBRANE POTENTIAL OF FROG SARTORIUS FIBERS [J].

LING, G ;

GERARD, RW .

JOURNAL OF CELLULAR AND COMPARATIVE PHYSIOLOGY, 1949, 34 (03) :383-396

[9]

Capillary-based droplet cells: limits and new aspects [J].

Lohrengel, MM ;

Moehring, A ;

Pilaski, M .

ELECTROCHIMICA ACTA, 2001, 47 (1-2) :137-141

[10]

Interface and volume effects in biological cells and electrochemical microcells [J].

Lohrengel, MM .

ELECTROCHIMICA ACTA, 1997, 42 (20-22) :3265-3271

← 1 2 3 →